Synthesis of Gold Nanoparticles Decorated with Multiwalled Carbon Nanotubes (Au-MWCNTs) via Cysteaminium Chloride Functionalization. View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2019-12

AUTHORS

Vu Duc Chinh, Giorgio Speranza, Claudio Migliaresi, Nguyen Van Chuc, Vu Minh Tan, Nguyen-Tri Phuong

ABSTRACT

Gold nanoparticles (AuNPs) decorated CNTs are promising materials for photocatalytics and biosensors. However, the synthesis of AuNPs chemically linked to the walls of MWCNTs is challenging and toxic products such as thionylchloride (SOCl2) or [1-ethyl-3(dimethyl-amino) propyl] carbodiimide hydrochloride (EDAC) need to be used. This work reports a new approach to prepare gold nanoparticles decorated multiwalled carbon nanotubes (MWCNTs) by using cysteaminium chloride via the formation of a Zwitterionic acide-base bond. The grafting process consists of 3 mains steps: oxidation, thiolation and decoration of AuNPs on the surface of MWCNTs. The completion of each step has been verified out by both spectroscopic (Raman, UV-Vis, FT-IR) and Scanning Electron Miscroscopy (SEM). The chemical bonding states of synthesized products have been proven by X-ray photoelectron spectroscopy (XPS). More... »

PAGES

5667

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/s41598-019-42055-7

DOI

http://dx.doi.org/10.1038/s41598-019-42055-7

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1113261521

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30952876


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