First Evidence for Mechanism of Inverse Ripening from In-situ TEM and Phase-Field Study of δ′ Precipitation in an Al-Li Alloy View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2019-12

AUTHORS

Jiwon Park, Reza Darvishi Kamachali, Sung-Dae Kim, Su-Hyeon Kim, Chang-Seok Oh, Christian Schwarze, Ingo Steinbach

ABSTRACT

In-situ TEM investigation of aging response in an Al-7.8 at.% Li was performed at 200 °C up to 13 hours. Semi-spherical δ' precipitates growing up to an average radius of 7.5 nm were observed. The size and number of individual precipitates were recorded over time and compared to large-scale phase-field simulations without and with a chemo-mechanical coupling effect, that is, concentration dependence of the elastic constants of the matrix solid solution phase. This type of coupling was recently reported in theoretical studies leading to an inverse ripening process where smaller precipitates grew at the expense of larger ones. Considering this chemo-mechanical coupling effect, the temporal evolution of number density, average radius, and size distribution of the precipitates observed in the in-situ experiment were explained. The results indicate that the mechanism of inverse ripening can be active in this case. Formation of dislocations and precipitate-free zones are discussed as possible disturbances to the chemo-mechanical coupling effect and consequent inverse ripening process. More... »

PAGES

3981

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/s41598-019-40685-5

DOI

http://dx.doi.org/10.1038/s41598-019-40685-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112641576

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30850676


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