Control of Multiferroic properties in BiFeO3 nanoparticles View Full Text


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Article Info

DATE

2019-12

AUTHORS

Diego Carranza-Celis, Alexander Cardona-Rodríguez, Jackeline Narváez, Oscar Moscoso-Londono, Diego Muraca, Marcelo Knobel, Nancy Ornelas-Soto, Andreas Reiber, Juan Gabriel Ramírez

ABSTRACT

BiFeO3 (BFO) nanoparticles (NPs) were synthesized using the sol-gel method at different calcination temperatures from 400 °C to 600 °C. XRD studies have confirmed that all BFO NPs show distorted rhombohedral crystals that match the R3c space group. We found evidence of local structural strain that develops with increasing particle size as suggested by TEM and Raman spectroscopy measurements. Magnetic measurements suggest that NPs have two distinct regimes: a ferromagnetic-like one at low temperatures and a superparamagnetic-like one at room temperature. The crossover temperature increases with NPs size, suggesting a size-dependent blocking magnetic regime. Similarly, local piezoelectric measurements at room temperature in single NP have confirmed a ferroelectric order with a NP size-dependent d33 coefficient. An analysis of both the ferroelectric and the magnetic results suggest that ferromagnetism and ferroelectricity coexist at room temperature in NPs. Our results lead to the possibility of tailoring the ferroic order in multifunctional materials by means of NP size. More... »

PAGES

3182

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/s41598-019-39517-3

DOI

http://dx.doi.org/10.1038/s41598-019-39517-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112433332

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30816194


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