In-Situ observation of local atomic structure of Al-Cu-Fe quasicrystal formation View Full Text


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Article Info

DATE

2019-12

AUTHORS

Hadi Parsamehr, Ying-Jiu Lu, Tzu-Ying Lin, An-Pang Tsai, Chih-Huang Lai

ABSTRACT

The phase and local environment, neighbouring atoms and coordination numbers (CN), for an Al-Cu-Fe multilayer were studied during heating (to 800 °C) and cooling (to room temperature) processes using in-situ X-Ray diffraction (XRD) and in-situ X-ray absorption spectroscopy (XAS) techniques to investigate the formation of Al-Cu-Fe quasicrystals (QCs). In-situ XRD clarified the transition of the ω-Al7Cu2Fe phase to a liquid state at the high temperature which transformed into the QC phase during cooling. The in-situ XAS showed a relatively small shift in distance between Cu-Al and Fe-Al during the phase evolution from RT to 700 °C. The distance between Cu-Cu, however, showed a significant increase from ω-phase at 700 °C to the liquid state at 800 °C, and this distance was maintained after QC formation. Furthermore, the CN of Fe-Al was changed to N = 9 during cooling. Through our observations of changes in CN, atomic distances and the atomic environment, we propose the local structural ordering of the quasicrystalline phase originated from a liquid state via ω-phase. In this study, we give a clear picture of the atomic environment from the crystalline to the quasicrystalline phase during the phase transitions, which provides a better understanding of the synthesis of functional QC nanomaterials. More... »

PAGES

1245

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/s41598-018-37644-x

DOI

http://dx.doi.org/10.1038/s41598-018-37644-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1111910206

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30718572


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