Zn-Nx sites on N-doped carbon for aerobic oxidative cleavage and esterification of C(CO)-C bonds View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2021-08-10

AUTHORS

Chao Xie, Longfei Lin, Liang Huang, Zixin Wang, Zhiwei Jiang, Zehui Zhang, Buxing Han

ABSTRACT

Selective cleavage of C-C bonds is very important in organic chemistry, but remains challenging because of their inert chemical nature. Herein, we report that Zn/NC-X catalysts, in which Zn2+ coordinate with N species on microporous N-doped carbon (NC) and X denotes the pyrolysis temperature, can effectively catalyze aerobic oxidative cleavage of C(CO)-C bonds and quantitatively convert acetophenone to methyl benzoate with a yield of 99% at 100 °C. The Zn/NC-950 can be applied for a wide scope of acetophenone derivatives as well as more challenging alkyl ketones. Detail mechanistic investigations reveal that the catalytic performance of Zn/NC-950 can be attributed to the coordination between Zn2+ and N species to change the electronic state of the metal, synergetic effect of the Zn single sites with their surrounding N atoms, as well as the microporous structure with the high surface area and structural defects of the NC. More... »

PAGES

4823

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/s41467-021-25118-0

DOI

http://dx.doi.org/10.1038/s41467-021-25118-0

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1140314099

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/34376654


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