Triamidoamine uranium(IV)–arsenic complexes containing one-, two- and threefold U–As bonding interactions View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2015-06-15

AUTHORS

Benedict M. Gardner, Gábor Balázs, Manfred Scheer, Floriana Tuna, Eric J. L. McInnes, Jonathan McMaster, William Lewis, Alexander J. Blake, Stephen T. Liddle

ABSTRACT

To further our fundamental understanding of the nature and extent of covalency in uranium–ligand bonding, and the benefits that this may have for the design of new ligands for nuclear waste separation, there is burgeoning interest in the nature of uranium complexes with soft- and multiple-bond-donor ligands. Despite this, there have so far been no examples of structurally authenticated molecular uranium–arsenic bonds under ambient conditions. Here, we report molecular uranium(IV)–arsenic complexes featuring formal single, double and triple U–As bonding interactions. Compound formulations are supported by a range of characterization techniques, and theoretical calculations suggest the presence of polarized covalent one-, two- and threefold bonding interactions between uranium and arsenic in parent arsenide [U–AsH2], terminal arsinidene [U=AsH] and arsenido [U≡AsK2] complexes, respectively. These studies inform our understanding of the bonding of actinides with soft donor ligands and may be of use in future ligand design in this area. More... »

PAGES

582-590

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/nchem.2279

DOI

http://dx.doi.org/10.1038/nchem.2279

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1035927646

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/26100807


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