Lithiacarboranes and 1,2,4-triazine 4-oxides: SNH reactions and ring transformations View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2004-06

AUTHORS

O. N. Chupakhin, A. M. Prokhorov, D. N. Kozhevnikov, V. L. Rusinov, I. A. Glukhov, Z. A. Starikova, V. A. Ol"shevskaya, V. N. Kalinin, M. Yu. Antipin

ABSTRACT

The reactions of 1-lithia-1,2- or 1,7-dicarba-closo-dodecaborane with 1,2,4-triazine 4-oxides can follow two competitive pathways: deoxygenative nucleophilic substitution of hydrogen to form 1-(1,2,4-triazin-5-yl)-1,2- or 1,7-dicarba-closo-dodecaboranes and the transformation of the 1,2,4-triazine ring into the triazoline ring giving rise to 1-(2-acetyl-1-aroyl-3-aryl-1,2,4-triazolin-5-yl)-1,2-dicarba-closo-dodecaboranes. Introduction of the electron-withdrawing triazine ring into the carborane cage substantially facilitates deboronation to give 1-(1,2,4-triazin-5-yl)-1,2-1,7-dicarba-nido-undecaboranes. More... »

PAGES

1223-1231

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/b:rucb.0000042277.99035.a8

DOI

http://dx.doi.org/10.1023/b:rucb.0000042277.99035.a8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1028487036


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