Syntheses and crystal structures of SmIII and ThIV complexes with macrocyclic cavitand cucurbituril View Full Text


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Article Info

DATE

2003-10

AUTHORS

D. G. Samsonenko, M. N. Sokolov, O. A. Gerasko, A. V. Virovets, J. Lipkowski, D. Fenske, V. P. Fedin

ABSTRACT

Slow evaporation of solutions of samarium nitrate and thorium chloride in hydrochloric acid containing the macrocyclic cavitand cucurbituril (C36H36N24O12) afforded crystals of the [{Sm(H2O)5(NO3)}2(C36H36N24O12)](NO3)4·6.5H2O and [{Th(H2O)5Cl}2(C36H36N24O12)]Cl6·13H2O complexes, respectively. The [Sm(C36H36N24O12)(H2O)5(SO4)][Sm(H2O)5(SO4)2]·17H2O complex was generated upon heating (130 °C) of a mixture of samarium sulfate, cucurbituril, and water in a sealed tube. X-ray diffraction analysis demonstrated that the metal atoms in these complexes are bound to the portal oxygen atoms of the cucurbituril molecules. In addition, the portal oxygen atoms of cucurbituril are linked to the coordinated H2O molecules via hydrogen bonds. More... »

PAGES

2132-2139

References to SciGraph publications

  • 1994-09. Cucurbituril: Supramolecular perspectives for an old ligand in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
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    http://dx.doi.org/10.1023/b:rucb.0000011868.74173.8d

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