Preparation of nanocrystalline SrBi2Ta2O9 powders using sucrose-PVA as the polymeric matrix View Full Text


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Article Info

DATE

2004-06

AUTHORS

A. B. Panda, A. Tarafdar, S. Sen, A. Pathak, P. Pramanik

ABSTRACT

Nanocrystalline powders of SrBi2Ta2O9 (Strontium Bismuth Tantalate) have been prepared through evaporation of a polymer-based aqueous precursor solution. The precursor solution was obtained by homogeneous dispersion of the water-soluble metal salts (i.e., strontium nitrate, bismuth nitrate and tartarate complex of tantalum) in a polymeric matrix created by an aqueous solution mixture of sucrose and polyvinyl alcohol. Complete evaporation of the precursor solution (at ∼200°C) resulted in a fluffy, porous, carbonaceous mass, which on calcination at 750°C/2 h yield the single-phase SrBi2Ta2O9 powders with average particle size ∼35 nm. The compacted powders, after sintering at 1000°C/4 h, show density of 96.8% of its theoretical value and dielectric constant value of 862 with Curie temperature (Tc) at 287°C, when measured at 100 KHz. More... »

PAGES

3739-3744

References to SciGraph publications

  • 1997-01. Alkoxide derived SrBi2Ta2O9 phase pure powder and thin films in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 1995-10. Synthesis of nano particle of inorganic oxides by polymer matrix in BULLETIN OF MATERIALS SCIENCE
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    http://scigraph.springernature.com/pub.10.1023/b:jmsc.0000030728.33285.61

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    http://dx.doi.org/10.1023/b:jmsc.0000030728.33285.61

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