Ontology type: schema:ScholarlyArticle
2003-06
AUTHORSM. A. Dapino, S. M. Cotes, A. F. Cabrera, R. C. Mercader, J. Desimoni
ABSTRACTIn this work we explore electrochemical-polishing for thinning Fe-Mn samples. We set out by studying with CEMS and XCMS a sample approximately 1 mm thick of a bcc Fe-13.7 wt.% Mn alloy, and subjected it to electrochemical etching in a solution of 10% perchloric acid and 90% acetic acid solution. Afterwards, the sample was electrochemically thinned to reach the suitable thickness to perform transmission Mössbauer spectroscopy. This technique is sensitive to the different Fe-Mn configurations of the bcc-Fe(Mn) substitutional solid solution whose relative populations depend on the Mn concentration. After analysing the spectra, and considering a random distribution approximation model, we discuss the conditions in which electrochemical polishing can be used as a reliable method for thinning this type of samples. More... »
PAGES331-336
http://scigraph.springernature.com/pub.10.1023/b:hype.0000003795.05473.5c
DOIhttp://dx.doi.org/10.1023/b:hype.0000003795.05473.5c
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