Complexation of Calix[4]arenephosphonous Acids with 2,4-Dichlorophenoxyacetic Acid and Atrazine in Water View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2003-06

AUTHORS

O.I. Kalchenko, A.V. Solovyov, S.A. Cherenok, N.F. Starodub, V.I. Kalchenko

ABSTRACT

Calix[4]arene phosphonous acids possessing two or four dihydroxyphosphoryl groups linked with the para-positions of the macrocyclic skeleton directly or by an aminomethyl spacer have been synthesised and their complexation with the herbicides2,4-dichlorophenoxyacetic acid (2,4-D) or atrazine (AT) in water has been investigated by the reversed phase HPLC method. The association constants of the 1 : 1 guest–host complexes of the herbicides (guest) with the calixarenes (host) in the range 772–5077 M-1 (2,4-D) and 2513–6785 M-1 (AT) have been determined from the relationship between the capacity factor of the guest and concentration of the calixarene host in the mobile phase. The association constants are dependent on the conformation and stereochemical mobility of the calixarene skeleton, the number of the dihydroxyphosphoryl groups at the upper rim, as well as the acid-base properties of the guest. Hydrophobic, electrostatic, and π-π-aromatic interactions in the guest–host complexes are discussed. More... »

PAGES

19-25

References to SciGraph publications

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URI

http://scigraph.springernature.com/pub.10.1023/a:1025626925863

DOI

http://dx.doi.org/10.1023/a:1025626925863

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https://app.dimensions.ai/details/publication/pub.1016482603


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