Reaction-induced phase separation in an epoxy/low molecular weight solvent system View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2003-07

AUTHORS

E. Soulé, M. García de la Mata, J. Borrajo, P. A. Oyanguren, M. J. Galante

ABSTRACT

Blends based on a stoichiometric mixture of diglycidyl ether of bisphenol A (DGEBA) and 2,2′-bis(4-amino-cyclohexyl)methane (ACHM) and cyclohexane as low molecular weight solvent were studied. The polymerization kinetics data experimentally obtained at different temperatures (30–60°C) were accurate fitted using a mechanistic model. The effect of the solvent over the polymerization rate was analyzed. No influence of the presence of the solvent was found up to 20 wt% of cyclohexane in the sample. The thermodynamic analysis using Flory-Huggins model allowed determination of the initial miscibility of binary blends containing DGEBA/cyclohexane and pseudo-binary mixtures of DGEBA/ACHM/cyclohexane. The presence of ACHM increases the DGEBA/cyclohexane initial solubility. The reaction-induced phase separation was described using a conversion-composition transformation phase diagram. It indicates that phase separation takes place by a nucleation and growth (NG) mechanism. The appropriate selection of composition of the blend and polymerization conditions led to final materials with a desired closed cell porous morphology. More... »

PAGES

2809-2814

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1024420132081

DOI

http://dx.doi.org/10.1023/a:1024420132081

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1029358161


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