Reaction of CpRu(PPh3)2Cl with six-member cyclothioethers. Structures of the [CpRu(PPh3)xL]Y complexes (L = pentamethylene sulfide, x = 2, Y = ... View Full Text


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Article Info

DATE

2003-06

AUTHORS

Mark Green, M. Draganjac, Yanjing Jiang, Paul M. Nave, A.W. Cordes, C.D. Bryan, J.K. Dixon, S.L. Folkert, C.-H. Yu

ABSTRACT

The synthesis of a series of ruthenium complexes with cyclothioether ligands is reported. The compounds were characterized by X-ray diffraction techniques. The molecular structures of [CpRu(PPh3)2(pms)]BF4 (1), [CpRu(PPh3)2(1,3-dithiane)]OTfl (2), [CpRu(PPh3)2(1,3,5-trithiane)]OTfl (3), and [CpRu(PPh3)(1,4-dithiane)]BF4 (4) show chelation occurs only when the sulfur atoms are separated by at least two C atoms, creating a ligand bite size large enough to chelate. Cell parameters: 1, space group P21/c, a = 14.601(4), b = 19.102(10), c = 14.751(7) Å, β = 98.28(3)○; 2, space group P21/c, a = 12.859(7), b = 15.576(3), c = 22.126(11) Å, β = 102.22(4)○; 3, space group P21/c, a = 12.7320(20), b = 15.571(5), c = 22.287(4) Å, β = 101.812(14)○; 4, space group Pbca, a = 11.2010(10), b = 16.321(7), c = 28.966(4) Å. Compounds 2 and 3 are X-ray isomorphous. The Ru–S bond lengths range from 2.341(3), 2.365(3) Å in compound 4 to 2.382(4) Å in compound 2. Upon chelation (compound 4), with subsequent loss of PPh3, the Ru–P bond shortens to 2.327(3) Å. This may be due to reduced steric hindrance about the Ru atom. No evidence for C–S bond lengthening is observed. More... »

PAGES

473-479

References to SciGraph publications

  • 1999-03. Synthesis and molecular structure of [CpRu(1,4,7-S3C6H12)]O3SCF3 in JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
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