Synthesis and crystal structures of sumpramolecular compounds of cucurbit[n]urils (n = 6, 8) with polynuclear strontium aqua complexes View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2003-03

AUTHORS

O. A. Gerasko, A. V. Virovets, D. G. Samsonenko, A. A. Tripol"skaya, V. P. Fedin, D. Fenske

ABSTRACT

Crystals of the {[Sr4(H2O)12(NO3)4](C36H36N24O12)}(NO3)4·3H2O and {[Sr2(H2O)12][Sr(H2O)3(NO3)2]2(C48H48N32O16)}(NO3)4·8H2O were prepared by slow concentration of aqueous solutions containing strontium nitrate and macrocyclic cavitands, viz., cucurbit[6]uril and cucurbit[8]uril ([C6H6N4O2]n, n = 6 and 8), respectively. According to the results of X-ray diffraction analysis, the crystal structures of these supramolecular compounds are built from polymeric chains, which consist of the alternating cucurbit[n]uril molecules and Sr2+ cations linked through the bridging aqua ligands and nitrate anions. The supramolecular compound of cucurbit[8]uril provides the first example of compounds in which this macrocycle is bound to metal aqua complexes. More... »

PAGES

585-593

References to SciGraph publications

  • 1994-09. Cucurbituril: Supramolecular perspectives for an old ligand in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
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