High-Temperature Evolution of SiC/C Products Derived from Preceramic Polymers View Full Text


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Article Info

DATE

1999-09

AUTHORS

N. I. Baklanova, V. N. Kulyukin, V. G. Kostrovsky, N. Z. Lyakhov, V. V. Terskikh, G. Yu Turkina, L. V. Zhilitskaya, O. G. Yarosh, M. G. Voronkov

ABSTRACT

The products formed during thermolysis of organosilicon polymers containing unsaturated carbon-carbon bonds have been studied within the temperature range 20–1700°C by means of XRD, 13C and 29Si MAS NMR, and Raman spectroscopy. These products are distinguished by their structural instability. A continuous evolution of the products formed during organic–inorganic thermal transformation involves (i) ordering of the local surroundings of silicon atoms, the formation of a silicon carbide crystalline phase, and the transition from β to α and (ii) consumption of carbon for the completion of silicon carbide formation, carbon phase formation, and ordering. More... »

PAGES

289-296

References to SciGraph publications

  • 1984-11. Creep behaviour and structural characterization at high temperatures of Nicalon SiC fibres in JOURNAL OF MATERIALS SCIENCE
  • 1987-02. Raman study of SiC fibres made from polycarbosilane in JOURNAL OF MATERIALS SCIENCE
  • 1990-09. Structural evolutions from polycarbosilane to SiC ceramic in JOURNAL OF MATERIALS SCIENCE
  • 1984-04. Thermal stability of SiC fibres (Nicalon®) in JOURNAL OF MATERIALS SCIENCE
  • 1996-10. Effect of thermal treatment on the reactivity of SiC-based fibres in JOURNAL OF MATERIALS SCIENCE
  • Identifiers

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    http://scigraph.springernature.com/pub.10.1023/a:1021821004155

    DOI

    http://dx.doi.org/10.1023/a:1021821004155

    DIMENSIONS

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