Synthesis and crystal structures of supramolecular adducts of molybdenum and tungsten selenide aqua complexes with macrocyclic cavitand cucurbituril View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2002-10

AUTHORS

O. A. Gerasko, A. V. Virovets, M. N. Sokolov, D. N. Dybtsev, A. V. Gerasimenko, D. Fenske, V. P. Fedin

ABSTRACT

The supramolecular compounds {[W3Se4Cl3(H2O)6]2[PyH⊂C36H36N24O12]}Cl3·18H2O (1) and {[Cl3SnMo3Se4Cl3(H2O)6][Cl3SnMo3Se4Cl2(H2O)7](C36H36N24O12)}Cl·26H2O (2) were isolated from solutions of the selenium-containing tungsten and molybdenum clusters [W3Se4(H2O)9]4+ and [Cl3SnMo3Se4(H2O)9]3+, respectively, and organic cavitand cucurbituril. X-ray diffraction analysis demonstrated that the macrocylcic cucurbituril molecule is coordinated on both sides by the cluster cations through the formation of complementary hydrogen bonds. Compound 1 has a chain structure stabilized by Se...Se interactions between the adjacent cluster cores. In compound 2, the bridging μ2-selenium atoms of the cluster fragment Mo3Se4 are coordinated to the tin atom of the SnCl3– ligand, thus losing the ability to be involved in Se...Se interactions. More... »

PAGES

1800-1805

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1021383914533

DOI

http://dx.doi.org/10.1023/a:1021383914533

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https://app.dimensions.ai/details/publication/pub.1006943496


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