Coke formation on an industrial reforming Pt–Sn/γ‐Al2O3 catalyst View Full Text


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Article Info

DATE

2000-04

AUTHORS

C.L. Li, O. Novaro, X. Bokhimi, E. Muñoz, J.L. Boldú, J.A. Wang, T. López, R. Gómez, N. Batina

ABSTRACT

The characterization of the coke deposited on an industrial Pt–Sn/γ‐Al2O3 catalyst, used in a continuous reforming process, was performed with AFM, XRD, FTIR, EPR, NMR, TG‐DTG and DTA techniques. Composition, structure and location of the coke on the catalyst were investigated. The coke was predominantly deposited on the catalyst surface and in the interstices between the catalyst particles. Its content increased along the reactor from top to bottom. Coke was deposited in the form of uniform films and clusters of three‐dimensional disks with diameters between 0.12 and 0.18 μm. It had a pseudo‐graphite structure produced by the dehydrogenation and polymerization of the aromatic precursor compounds. The coked catalyst showed a good combustion behavior; it was regenerated below 550°C. These results are important to elucidate the coke formation mechanism, to generate new continuous reforming catalysts, and to optimize the reactor operation parameters. More... »

PAGES

209-216

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1019042027077

DOI

http://dx.doi.org/10.1023/a:1019042027077

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178 grid-institutes:grid.418275.d schema:alternateName Laboratory of Catalysis and Materials, Superior School of Chemical Engineering (ESIQIE), National Polytechnic Institute of Mexico (IPN), Zacatenco, UPALM, 07738, Mexico City, Mexico
179 schema:name Laboratory of Catalysis and Materials, Superior School of Chemical Engineering (ESIQIE), National Polytechnic Institute of Mexico (IPN), Zacatenco, UPALM, 07738, Mexico City, Mexico
180 rdf:type schema:Organization
181 grid-institutes:grid.7220.7 schema:alternateName Department of Chemistry, Universidad Autónoma Metropolitana‐I, A.P. 55‐534, 09340, México D.F., Mexico
182 schema:name Department of Chemistry, Universidad Autónoma Metropolitana‐I, A.P. 55‐534, 09340, México D.F., Mexico
183 rdf:type schema:Organization
 




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