Reactions of the Cluster Anion [HRu3(CO)11)]− with Dicyclohexylphosphine: Synthesis and Molecular Structure of H2Ru3(CO)8(PCy2)2 and H2Ru3(CO)6(PCy2)2(HPCy2)2 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2001-03

AUTHORS

Georg Süss-Fink, Isabelle Godefroy, Matthieu Faure, Antonia Neels, Helen Stoeckli-Evans

ABSTRACT

The cluster anion [HRu3(CO)11]- (1) reacts with dicyclohexylphosphine in THF solution to give the anionic derivative [HRu3(CO)8(PCy2)2]- (2), protonation of which yields the neutral cluster H2Ru3(CO)8(PCy2)2 (3) and, in the presence of excess phosphine, HRu3(CO)7(PCy2)3 (4). In protic methanol as reaction medium, the reaction of 1 with HPCy2 gives directly the neutral complex H2Ru3(CO)6(PCy2)2(HPCy2)2 (5), together with 4. The single-crystal structure X-ray analysis of 3 shows a closed triangular Ru3 framework. The electron count is in accordance with the EAN rule, but the structure analysis of 5 reveals an open, almost linear Ru3 skeleton, which is electron-deficient with respect to the EAN rule. More... »

PAGES

35-48

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1016610709985

DOI

http://dx.doi.org/10.1023/a:1016610709985

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1014528621


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