Organic/Inorganic Hybrid Materials Based on Silsesquioxanes Derived from (3-Methacryloxypropyl) Trimethoxysilane and Their Blends with Vinylester Resins View Full Text


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Article Info

DATE

2002-01

AUTHORS

M.A. Fanovich, S.A. Pellice, P.G. Galliano, R.J.J. Williams

ABSTRACT

The crosslinking of blends of a silsesquioxane (SSO) derived from (3-methacryloxypropyl) trimethoxysilane, variable amounts of a vinylester resin (VE, dimethacrylate of bisphenol A), and benzoyl peroxide (BPO) or dicumyl peroxide (DCP) as initiators, was followed by differential scanning calorimetry (DSC). For the neat SSO a thermally-initiated polymerization was observed in the 150–250°C range, leading to a conversion close to 22% of the initial C=C groups. The final conversion could be increased to a maximum value close to 83%, by adding an initiator and using a thermal cycle attaining temperatures in the range of 200°C. The use of variable amounts of VE as a co-monomer produced a slight increase of the final conversion in SSO/VE/BPO blends. Neither the conversion of double-bonds nor the addition of the VE had any effect on the onset temperature of thermal degradation, which was associated to the presence of the methacryloxypropyl groups supplied by the SSO and the VE resin. However, a distinct two-step degradation process was observed in the presence of VE. Coatings based on SSO/VE/BPO blends exhibited more uniform thicknesses and lower values of the microhardness than those devoid of VE. However, the conversion of C=C groups did not show any significant effect on the values of microhardness. More... »

PAGES

45-52

References to SciGraph publications

  • 1994-01. Functional coatings on glass using ORMOCER®-systems in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 1994-01. Characterization of the hydrolysis and polymerization processes of methacryloxypropyltrimethoxysilane in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 1994-01. The influence of methacryloxypropyltrimethoxysilane on the sol-gel process of TEOS in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 1994-01. A two-component, non-aqueous route to silica gel in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1023/a:1013323819913

    DOI

    http://dx.doi.org/10.1023/a:1013323819913

    DIMENSIONS

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