Calorimetry under Stress A Preliminary Study in Single Crystalline Cu-Zn-Al Shape Memory Alloys View Full Text


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Article Info

DATE

1999-07

AUTHORS

J. L. Pelegrina, M. Sade, C. Auguet, V. Torra, A. Torralba

ABSTRACT

A non-differential calorimetric analyzer was developed for an INSTRON 1123 machine (a stress-strain-temperature analyzer) with a temperature chamber INSTRON 1110. The study was performed using the Joule effect and pseudoelastic martensitic transformations in single crystals of Cu-Zn-Al alloys. The analysis of the system establishes that: the sensitivity of calorimetric measurements after a filter of two poles and two zeros is 166 mV W-1 (at 297 K), the noise is near 1.5 μV and the drift is close to 30 μV in 6 h. The reproducibility of the sensitivity working with one sample is better than ±0.3%, and the change to a new sample keeps the value below ±0.5%. The uncertainty in reproducibility in the martensitic transformation (including repositioning) does not overcome ±1.6%. The used calorimetric sensors limit the temperature to 373 K. The furnace control originated fluctuations on the base line (near ±20 μV), which by means of an auxiliary signal processing were reduced to 50% (less than ±10 μV). More... »

PAGES

247-259

References to SciGraph publications

  • 1990-07. Improvements in calorimetry and thermal analysis applied to shape-memory alloys in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1023/a:1010113609505

    DOI

    http://dx.doi.org/10.1023/a:1010113609505

    DIMENSIONS

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