A comparative CP/MAS 13C-NMR study of cellulose structure in spruce wood and kraft pulp View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2000-03

AUTHORS

Eva-Lena Hult, Per Tomas Larsson, Tommy Iversen

ABSTRACT

CP/MAS 13C-NMR spectroscopy in combination with spectral fitting was used to study the supermolecular structure of the cellulose fibril in spruce wood and spruce kraft pulp. During pulping, structures contributing to inaccessible surfaces in the wood cellulose are converted to the cellulose Iβ allomorph, that is, the degree of order is increased. This increase is also accompanied by a conversion of cellulose Iα to cellulose Iβ. Cellulose from wood composed of different cell types, that is, compression wood, juvenile wood, earlywood, latewood and normal wood exhibited a similar supermolecular structure. Assignments were made for signals from hemicellulose which contribute significantly to the spectral C-4 region (80–86 ppm) in kraft pulp spectra but substantially less to the corresponding region in wood spectra. More... »

PAGES

35-55

Journal

TITLE

Cellulose

ISSUE

1

VOLUME

7

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1009236932134

DOI

http://dx.doi.org/10.1023/a:1009236932134

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1038980198


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