Hydroxyls nests in defective silicalites and strained structures derived upon dehydroxylation: vibrational properties and theoretical modelling View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2001-01

AUTHORS

S. Bordiga, P. Ugliengo, A. Damin, C. Lamberti, G. Spoto, A. Zecchina, G. Spanò, R. Buzzoni, L. Dalloro, F. Rivetti

ABSTRACT

Defective silicalite, an efficient and selective catalyst in the gas phase Beckmann rearrangement reaction, has been characterised by infrared spectroscopy and by molecular modelling techniques. We report a detailed IR study on the effect of outgassing treatments at increasing temperature on silanols bands and on framework modes. The effect of a temperature decrease up to 100 K (during the IR measurement) on the H-bonding interactions has also been investigated. The interaction of silanols with mesitylene, a probe molecule which cannot penetrate the channels, has been studied in order to distinguish between internal and external OH groups. Molecular mechanics and ab initio methods have also been used to model the structure and the vibrational features of a properly designed nest in order to support the assignments of the IR spectrum. More... »

PAGES

43-52

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1009019829376

DOI

http://dx.doi.org/10.1023/a:1009019829376

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1038045937


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