A Water Rich Crystalline Hydrate Formed by 1,4,7,10-Tetraazacyclododecane, Siliconhydrofluoric Acid and Water: Structure and Properties View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1998-03

AUTHORS

Marina S. Fonari, Yurii A. Simonov, Victor Ch. Kravtsov, Vladimir O. Gelmboldt, Edward V. Ganin, Yurii A. Popkov, Larisa V. Ostapchuk

ABSTRACT

Novel complementary associations have been found in a crystalline ternarycomplex of the macrocyclic tetramine, [12]aneN4 (e.g. =1,4,7,10-tetraazacyclododecane, cyclen, L), hexafluorosilicate ions andwater (I). The final compound belongs to the host—guest type with themacrocycle as the host (H), the inorganic entity as a guest (G) and watermolecules. It was characterized by X-ray techniques, IR spectroscopy andthermogravimetric study. X-ray crystal analysis revealed that the structureis built of the charged entities, with a 3D-network uniting thequadriprotonated form of the macrocycle, hexafluorosilicate as counterionsand lattice water molecules viaN—H+...F-,N—H+...O(w),OH...F- and O—-H(w)...O(w)hydrogen bonds. The overall complex stoichiometry comprises fourSiF62- anions and seven water molecules per two[LH4]4+ cations. Crystals of (I) are monoclinic,space group P21/n with a = 14.585(3), b = 16.384(2), c =16.500(3) Å, β = 92.84(3)°, V = 3938(1)Å3 and Z = 8 forC8H31F12N4O3.5Si2. More... »

PAGES

197-213

Identifiers

URI

http://scigraph.springernature.com/pub.10.1023/a:1007932615687

DOI

http://dx.doi.org/10.1023/a:1007932615687

DIMENSIONS

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