Strategies for the analysis of poly(methacrylic acid) by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2007-08

AUTHORS

Mark F. Wyatt, Nicolas Schaeffer, Bien Tan, Andrew I. Cooper

ABSTRACT

We evaluated several aqueous-based sample preparation protocols for the analysis of poly(methacrylic acid) (PMAA) by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOFMS). The sample contained a pentaerythritol tetra(3-mercaptopropionate) end-group, and was characterized in positive and negative ion modes using 2,5-dihydroxybenzoic acid (DHB) and 2,4,6-trihydroxyacetophenone (THAP) matrices. The major series observed were the [M + Na](+) species, in positive ion mode, and the [M - H](-) species, in negative ion mode. The performance of DHB and THAP matrices was comparable in positive ion mode, but THAP outperformed DHB in negative ion mode. The use of ion-exchange beads (IXB) benefited the analysis, while the addition of sodium acetate (NaOAc) or trifluoroacetic acid (TFA) proved disadvantageous in positive ion mode. More... »

PAGES

1507-1510

Identifiers

URI

http://scigraph.springernature.com/pub.10.1016/j.jasms.2007.05.015

DOI

http://dx.doi.org/10.1016/j.jasms.2007.05.015

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1001400904

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/17583530


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