Identification of a new source of interference leached from polypropylene tubes in mass-selective analysis View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2005-03

AUTHORS

Yuan-Qing Xia, Shefali Patel, Ray Bakhtiar, Ronald B. Franklin, George A. Doss

ABSTRACT

An interference leached from polypropylene tubes was identified to be a sulfoxide oxidative product of didodecyl 3,3'-thiodipropionate (DDTDP) that is used to prevent oxidative degradation of synthetic polymers. A sulfone oxidative product of DDTDP leached from the polypropylene tubes was also observed. The interfering compounds were isolated by LC and characterized using time-of-flight mass spectrometry and NMR. Authentic sulfoxide and sulfone products of DDTDP were also prepared by reacting DDTDP with hydrogen peroxide reaching an unequivocal structural assignment. In conclusion, when analytes of interest are solubilized in predominantly organic solvents and kept in polypropylene containers, the possibility of contamination from leached chemicals should be taken into account. More... »

PAGES

417-421

References to SciGraph publications

  • 2002-08. Plasticizer contamination from vacuum system o-rings in a quadrupole ion trap mass spectrometer in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1016/j.jasms.2004.11.020

    DOI

    http://dx.doi.org/10.1016/j.jasms.2004.11.020

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1044334079

    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/15734336


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