Effect of Gd3+ doping on structural and photocatalytic properties of ZnO obtained by facile microwave-hydrothermal method View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-04

AUTHORS

Juliane Z. Marinho, Leonardo F. de Paula, Elson Longo, Antonio O. T. Patrocinio, Renata C. Lima

ABSTRACT

Gd3+-doped ZnO nanoparticles with different Gd3+ concentrations were synthesized by an eco-friendly microwave hydrothermal method. X-ray diffraction measurements confirm that the prepared nanoplates exhibit hexagonal wurtzite structure. Gd3+ doping induces lattice expansion of ZnO due to the larger ionic radius of rare earth Gd3+ in relation to Zn2+ ions. Rietveld refinement, Raman and Photoluminescence (PL) spectra confirm that Gd3+ ions were successfully inserted into ZnO lattice. The 2.0 mol% Gd3+ doped sample exhibits an increased photoluminescence intensity in comparison to that for the undoped ZnO, which is attributed to the enhance in the defect concentration due to Gd3+ doping. The photocatalytic activities of the samples were also evaluated towards UV-A induced degradation of methylene blue in aqueous solution. The highest photocatalytic activity was observed for 1.0 mol% Gd3+-doped ZnO nanoparticles (73% for methylene blue degradation within 150 min under UV–Vis irradiation). The particles size, agglomeration degree and the electronic effects due to the Gd3+ dopping seems to be the main parameters that affect the photocatalytic activity of Gd3+-doped ZnO nanoparticles. More... »

PAGES

359

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s42452-019-0359-x

DOI

http://dx.doi.org/10.1007/s42452-019-0359-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112989131


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