Anodic stripping voltammetry studies of electrochemically engineered silver nanoparticles over single polypyrrole nanowire device for tracing of arsenic(III): an environmental ... View Full Text


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Article Info

DATE

2018-12

AUTHORS

Rahul S. Salunke, Padmakar G. Chavan, Dhammanand J. Shirale

ABSTRACT

Electrochemical detection of arsenic in adulterated water using single polypyrrole nanowire (PpyNW) decorated with silver nanoparticles (AgNPs) is reported. The PpyNWs were prepared with a template directed technique and aligned in between the gold pair of electrodes (1–2 μm gap) using an electrophoretic alignment method. The AgNPs were decorated on to the single PpyNW using cyclic voltammetry. The arsenic detection was done using anodic stripping voltammetry. The aligned PpyNW and decorated AgNPs were confirmed by scanning electron microscope and energy-dispersive spectroscopy technique. The improved sensitivity may be due to the discrete energy levels of nanowire co-related to aspect ratio and the nanoparticles. The limit of detection for PpyNW/AgNPs electrode is found to be 1.5 ppb, and the sensitivity of the sensor is recorded to 2.81 μA/ppb. The precision and sensitivity of the device enable to protect anti-arsenic domestic applications. More... »

PAGES

12

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http://scigraph.springernature.com/pub.10.1007/s41204-018-0042-2

DOI

http://dx.doi.org/10.1007/s41204-018-0042-2

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47 schema:description Electrochemical detection of arsenic in adulterated water using single polypyrrole nanowire (PpyNW) decorated with silver nanoparticles (AgNPs) is reported. The PpyNWs were prepared with a template directed technique and aligned in between the gold pair of electrodes (1–2 μm gap) using an electrophoretic alignment method. The AgNPs were decorated on to the single PpyNW using cyclic voltammetry. The arsenic detection was done using anodic stripping voltammetry. The aligned PpyNW and decorated AgNPs were confirmed by scanning electron microscope and energy-dispersive spectroscopy technique. The improved sensitivity may be due to the discrete energy levels of nanowire co-related to aspect ratio and the nanoparticles. The limit of detection for PpyNW/AgNPs electrode is found to be 1.5 ppb, and the sensitivity of the sensor is recorded to 2.81 μA/ppb. The precision and sensitivity of the device enable to protect anti-arsenic domestic applications.
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