Synthesis of 2,3,4,5-tetrasubstituted pyrroles and 1,4-dihydro-tetraarylpyrazines using acidic alumina as a heterogeneous catalyst View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-11

AUTHORS

Khodabakhsh Niknam, Hashem Sharghi, Mohsen Khataminejad

ABSTRACT

Some new 2,3,4,5-tetrasubstituted pyrroles were synthesized via three-component condensation reaction of benzoin derivatives, 1,3-dicarbonyl compounds, and ammonium acetate using acidic Al2O3 as an efficient and reusable heterogeneous catalyst in refluxing ethanol in high yields. Also, acidic alumina was catalyzed 1,4-dihydro-tetraarylpyrazines by the condensation reaction of benzoins and ammonium acetate in refluxing ethanol in high yields. Alumina showed much the same efficiency when used in consecutive reaction runs. Acidic alumina was used as heterogeneous acidic catalyst for the synthesis of tetrasubstituted pyrroles in refluxing ethanol. The catalyst could be recycled for several times. More... »

PAGES

1953-1961

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s13738-016-0912-0

DOI

http://dx.doi.org/10.1007/s13738-016-0912-0

DIMENSIONS

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47 schema:description Some new 2,3,4,5-tetrasubstituted pyrroles were synthesized via three-component condensation reaction of benzoin derivatives, 1,3-dicarbonyl compounds, and ammonium acetate using acidic Al2O3 as an efficient and reusable heterogeneous catalyst in refluxing ethanol in high yields. Also, acidic alumina was catalyzed 1,4-dihydro-tetraarylpyrazines by the condensation reaction of benzoins and ammonium acetate in refluxing ethanol in high yields. Alumina showed much the same efficiency when used in consecutive reaction runs. Acidic alumina was used as heterogeneous acidic catalyst for the synthesis of tetrasubstituted pyrroles in refluxing ethanol. The catalyst could be recycled for several times.
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