Immobilized palladium nanoparticles on silica functionalized N-propylpiperazine sodium N-propionate (SBPPSP): catalytic activity evaluation in copper-free Sonogashira reaction View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-12

AUTHORS

Khodabakhsh Niknam, Abdollah Deris, Farhad Panahi, M. Reza Hormozi Nezhad

ABSTRACT

An efficient heterogeneous palladium catalyst system has been developed based on immobilization of Pd nanoparticles on silica-bonded N-propylpiperazine sodium N-propionate (SBPPSP) substrate. SBPPSP substrate can stabilize the Pd nanoparticles effectively so that it can improve their stability against aggregation. In addition, grafted piperazine species on to the silica backbone prevent the removing of Pd nanoparticles from the substrate surface. Transmission electron microscopy (TEM) of catalyst is shown the size of Pd nanoparticles, also it confirmed by particle size analyzer which shown the average size of 21 nm for Pd. The catalytic activity of these catalysts was investigated in the Sonogashira reaction. The catalyst could be recycled several times without appreciable loss in catalytic activity. More... »

PAGES

1291-1296

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s13738-013-0271-z

DOI

http://dx.doi.org/10.1007/s13738-013-0271-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1032386590


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