Modification of an Electroplated Nickel Interlayer Surface by Annealing Heat Treatment for Diamond Deposition on Tungsten Carbide View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-01-03

AUTHORS

A. W. Hassan, M. Y. Noordin, S. Izman, K. Denni, E. M. Nazim

ABSTRACT

The tungsten carbide (WC-6%Co) substrate was coated with a nickel layer using the electrochemical deposition process to suppress cobalt diffusion during diamond deposition. However, the high solubility of nickel for carbon is a major issue, which hinders diamond nucleation and growth. Annealing heat treatment was conducted on the Ni/WC-6%Co specimens to reduce the interlayer solubility for carbon and enable diamond deposition. The heat treatment process was carried out inside a high-temperature tube furnace at two different temperatures (1050 and 850 °C) for a 60-min duration. Diamond was then deposited on the electroplated and heat-treated samples in a hot filament CVD reactor. Field emission electron microscopy, energy-dispersive spectroscopy, and X-ray diffraction analyzing techniques were used to characterize the heat-treated and diamond-coated samples. The results show that the annealing process could successfully modify the nickel-coated surface composition by the diffusion of tungsten. In addition, the annealed interlayer was able to suppress cobalt diffusion and promote the nucleation and growth of a continuous diamond film on the tungsten carbide substrate. More... »

PAGES

201-211

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s13632-018-0512-8

DOI

http://dx.doi.org/10.1007/s13632-018-0512-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1111100930


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