Gas-Phase Arylmethyl Transfer and Cyclodeamination of Argentinated N-Arylmethyl-Pyridin-2-Ylmethanimine View Full Text


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Article Info

DATE

2014-02

AUTHORS

Hezhi Sun, Lin Wang, Yuanjiang Pan

ABSTRACT

In collisional activation of argentinated N-arylmethyl-pyridin-2-ylmethanimine, a neutral molecule of AgNH2 is eliminated, carrying one hydrogen from the methylene and the other one from the ortho position (relative to the ipso carbon) of the aryl ring. Taking argentinated N-benzyl-pyridin-2-ylmethanimine for example, the proposition that the AgNH2 loss results from intramolecular arylmethyl transfer combined with cyclodeamination is rationalized by deuterium labeling experiments, blocking experiments, and theoretical calculations. The structure of the final product ion from loss of AgNH2 was confirmed further by multistage mass spectrometry. More... »

PAGES

169-175

References to SciGraph publications

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    URI

    http://scigraph.springernature.com/pub.10.1007/s13361-013-0778-7

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    http://dx.doi.org/10.1007/s13361-013-0778-7

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    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/24356863


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