Surface Acoustic Wave Nebulization Produces Ions with Lower Internal Energy than Electrospray Ionization View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2012-04-03

AUTHORS

Yue Huang, Sung Hwan Yoon, Scott R. Heron, Christophe D. Masselon, J. Scott Edgar, František Tureček, David R. Goodlett

ABSTRACT

Surface acoustic wave nebulization (SAWN) has recently been reported as a novel method to transfer non-volatile analytes directly from solution to the gas phase for mass spectrometric analysis. Here we present a comparison of the survival yield of SAWN versus electrospray ionization (ESI) produced ions. A series of substituted benzylpyridinium (BzPy) compounds were utilized to measure ion survival yield from which ion energetics were inferred. We also estimated bond dissociation energies using higher level quantum chemical calculations than previously reported for BzPy ions. Additionally, the effects on BzPy precursor ion survival of SAWN operational parameters such as inlet capillary temperature and solution flow-rate were investigated. Under all conditions tested, SAWN-generated BzPy ions displayed a higher tendency for survival and thus have lower internal energies than those formed by ESI. More... »

PAGES

1062-1070

References to SciGraph publications

  • 2003-03. Mass spectrometry-based proteomics in NATURE
  • 2010-01. Fragmentation of benzylpyridinium “thermometer” ions and its effect on the accuracy of internal energy calibration in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • 2007-03-01. Shrinking droplets in electrospray ionization and their influence on chemical equilibria in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • 1999-04-01. Nanoelectrospray—More than just a minimized-flow electrospray ionization source in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • 2010-01-28. Comparison of the internal energy deposition of direct analysis in real time and electrospray ionization time-of-flight mass spectrometry in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • 2008-02-12. Surface acoustic wave biosensors: a review in ANALYTICAL AND BIOANALYTICAL CHEMISTRY
  • 2008-03. Internal energy distributions in desorption electrospray ionization (DESI) in JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s13361-012-0352-8

    DOI

    http://dx.doi.org/10.1007/s13361-012-0352-8

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1004082655

    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/22476889


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