Synthesis and Characterization of a Lateral Phthalonitrile Functionalized Main-Chain Polybenzoxazine Precursor View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-05

AUTHORS

Jian Zheng, Yan Zhang, Ying Wang, Jianqun Gan, Lu Shen, FuBin Luo, Liyan Liang, Kun Wu, Mangeng Lu

ABSTRACT

A lateral phthalonitrile functionalized main-chain polybenzoxazine precursor has been successfully synthesized. The structure was characterized by proton nuclear magnetic resonance (1H NMR) and Fourier transform infrared (FTIR). The formation of benzoxazine rings were confirmed by the characteristic resonances observed at about 4.55 (C-CH2-N) and 5.30 ppm (N-CH2-O) and the absorbance at 950 cm-1 of benzene attached with an oxazine ring. The curing behavior was monitored by differential scanning calorimetry (DSC) and in situ FTIR. The completion of polymerization was proved by the disappearance of the band located at 950 cm-1 in FTIR. Thermogravimetric analysis (TGA) was used to investigate the thermal stability, and the results indicated that the thermal stability of the cured polymer gained significant improvement than that without phthalonitrile functionalization. More... »

PAGES

409-414

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s13233-016-4061-1

DOI

http://dx.doi.org/10.1007/s13233-016-4061-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1052357196


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