Lipase catalyzed reaction of L-ascorbic acid with cinnamic acid esters and substituted cinnamic acids View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-02

AUTHORS

Yung-Hun Yang, Takao Raku, Eunjung Song, Sung-Hee Park, Dongwon Yoo, Hyung-Yeon Park, Byung-Gee Kim, Hyung-Ju Kim, Sang-Hyun Lee, Hyung-Sup Kim, Yutaka Tokiwa

ABSTRACT

To perform the lipase-catalyzed synthesis of L-ascorbic acid derivatives from plant-based compounds such as cinnamic and ferulic acid under mild reaction conditions, the activities of immobilized Candida ntarctica lipase with different cinnamic acid esters and substituted cinnamic acids were compared. As a result, immobilized C. ntarctica lipase was found to prefer vinyl cinnamic acid to other esters such as allyl-, ethyl-, and isobutyl cinnamic acids as well as substituted cinnamic acids such as p-coumaric acid, caffeic acid, ferulic acid, and sinapic acid. Based on these results, large-scale synthesis of 6-O-cinnamyl-L-ascorbic acid ester was performed using immobilized C. ntarctica lipase in dry organic solvent, resulting in 68% yield (493 mg) as confirmed by 13C-NMR. More... »

PAGES

50-54

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s12257-011-0071-1

DOI

http://dx.doi.org/10.1007/s12257-011-0071-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1010671727


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