Synthesis, characterization and superoxide dismutase activity of bi-copper(II)-bisacetato- μ−phthalicacid[bis(benzyloxy)ethyl]ester View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-03

AUTHORS

BABITA SARMA, PRADIP K BHATTACHARYYA, DIGANTA KUMAR DAS

ABSTRACT

A new binuclear copper(II) complex, bridged by the ligand phthalicacid[bis(benzyloxy)ethyl]ester, where each copper(II) is coordinated to one carboxylate (from ligand) and one acetate in square planar mode is reported. The ligand synthesized by the reaction of phthalic anhydride and ethylene glycol, has been characterized by FT-IR, 1HNMR and LCMS. The binuclear Copper(II) complex has been characterized by UV/visible spectra, FTIR spectra, EPR spectra, ESI-MS spectra, magnetic moment measurement and thermogravimetric analysis. DFT calculation has shown a Z type structure for the complex. Excellent superoxide dismutase activity with IC50 value 8.6 ×10−6 M for the complex has been observed. Graphical AbstractA new binuclear copper(II) complex, bridged by the ligand phthalicacid[bis (benzyloxy)ethyl]ester, where each copper(II) is coordinated to one carboxylate (from ligand) and one acetate in square planar mode is reported. A new binuclear copper(II) complex, bridged by the ligand phthalicacid[bis (benzyloxy)ethyl]ester, where each copper(II) is coordinated to one carboxylate (from ligand) and one acetate in square planar mode is reported. More... »

PAGES

455-459

Journal

TITLE

Journal of Chemical Sciences

ISSUE

3

VOLUME

127

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s12039-015-0798-x

DOI

http://dx.doi.org/10.1007/s12039-015-0798-x

DIMENSIONS

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