Pyrene appended bile acid conjugates: Synthesis and a structure–gelation property study View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2011-07

AUTHORS

SHREEDHAR BHAT, ARTO VALKONEN, JUHA KOIVUKORPI, ANUPAMA AMBIKA, ERKKI KOLEHMAINEN, UDAY MAITRA, KARI RISSANEN

ABSTRACT

A wide variety of novel compounds obtained by combining two types of known organogelators, viz., bile acid alkyl amides and pyrene alkanoic acids, were synthesized and screened for their gelation ability. The 3α esters of 1-pyrene butyric acid (PBA) of alkylamides of deoxycholic acid (DCA) turned out to be effective in the gel formation with many organic solvents although the gelation has to be triggered by the addition of a charge transfer (CT) agent 2,4,7-trinitrofluorenone (TNF). The special feature of these molecules is that the organogelation is achieved only after derivatizing the acid moiety of the 1-pyrenealkanoic acids. Additionally, the gelation properties can be fine-tuned by inserting different functional groups at the bile acid side chain. The gels obtained are deep red in colour and optically transparent up to 2% w/v. The SEM studies of the obtained xerogels revealed bundled rod-like morphology without specialized branching. Graphical AbstractCharge-transfer interaction promoted organogelation has been observed with a number of pyrene appended bile acid conjugates in the presence of trinitrofluorenone. Charge-transfer interaction promoted organogelation has been observed with a number of pyrene appended bile acid conjugates in the presence of trinitrofluorenone. More... »

PAGES

379-391

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s12039-011-0100-9

DOI

http://dx.doi.org/10.1007/s12039-011-0100-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1049003825


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