Equilibrium and crystallographic measurements of the binary tetrahydrofuran and helium clathrate hydrates View Full Text


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Article Info

DATE

2008-01

AUTHORS

Sun-Hwa Yeon, Jeasung Park, Youngjune Park, Sukjeong Choi, Kyuchul Shin, Jiwoong Seol, Minjun Cha, Huen Lee

ABSTRACT

Clathrate compounds are crystalline materials formed by a physical interaction between host and relatively light guest molecules. Various types of nano-sized cages surrounded by host frameworks exist in the highly unique crystalline structures and free guest molecules are entrapped in an open host-guest network. Recently, we reported two peculiar phenomena, swapping and tuning, naturally occurring in the hydrate cages. Helium, one of the smallest light guest molecules, must be the challengeable material in the sense of physics and moreover possesses versatile applications in the field of superconductivity technology and thermonuclear industry. In this regard, we attempted for the first time to synthesize helium hydrates at moderate temperature and pressure conditions. According to inclusion phenomena, helium itself normally cannot form clathrate hydrates due to being too small molecularly without the help of hydrate former molecules (sI, sII, and sH formers). In this study, the hydrate equilibria of the binary clathrate hydrate containing tetrahydrofuran, helium, and water were determined at 2, 3, 5.56 THF mol%. Direct volumetric measurements were also carried out to confirm the exact amount of helium captured in the hydrate cages. Finally, the crystalline structure of the formed mixed hydrates was identified by powder X-ray diffraction, resulting in structure II. More... »

PAGES

154-157

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http://scigraph.springernature.com/pub.10.1007/s11814-008-0028-z

DOI

http://dx.doi.org/10.1007/s11814-008-0028-z

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132 schema:name Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology, 373-1 Guseong-dong, Yuseong-gu, 305-701, Daejeon, Korea
133 rdf:type schema:Organization
 




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