Preparation of ferromagnetic metal fine fibers by organic gel-thermal reduction process View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-10-01

AUTHORS

Kai Cao, Xiang-qian Shen, Mao-xiang Jing, Jian-xin Zhou

ABSTRACT

The organic gel-thermal reduction process was used for the preparation of ferromagnetic metal Ni, Co and Fe fine fibers from the raw materials of citric acid, lactic acid and metal salts. The structure, thermal decomposition process and morphologies of the gel precursors and fibers derived from thermal reduction of these gel precursors were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, thermo-gravimetric/differential scanning calorimetry and scanning electron microscopy. The results show that spinnability of gel largely depends on molecular structure of metal-carboxylate complex that is a linear-type structure formed in the gel. As a result, the gels exhibit a good spinnability. Metal Ni, Co and Fe fine fibers are featured with diameters of around 1 μm and a high aspect ratio up to 1 × 106. More... »

PAGES

607-611

References to SciGraph publications

  • 2002-09. Electrophoretic deposition of alkaline earth coatings from EDTA complexes in JOURNAL OF MATERIALS SCIENCE
  • 2007-06-01. Synthesis and characterization of Cu-Cr-O nanocomposites in JOURNAL OF CENTRAL SOUTH UNIVERSITY
  • 2000-11. Preparation of alkaline earth carbonates and oxides by the EDTA-gel process in JOURNAL OF MATERIALS SCIENCE
  • 2000-04. Submicron diameter nickel filaments and their polymer-matrix composites in JOURNAL OF MATERIALS SCIENCE
  • 2004-12-01. Preparation of copper nano-wires by template synthesis method in JOURNAL OF CENTRAL SOUTH UNIVERSITY
  • 2000-06. Materials for electromagnetic interference shielding in JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s11771-007-0116-y

    DOI

    http://dx.doi.org/10.1007/s11771-007-0116-y

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1046638547


    Indexing Status Check whether this publication has been indexed by Scopus and Web Of Science using the SN Indexing Status Tool
    Incoming Citations Browse incoming citations for this publication using opencitations.net

    JSON-LD is the canonical representation for SciGraph data.

    TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

    [
      {
        "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
        "about": [
          {
            "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/09", 
            "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
            "name": "Engineering", 
            "type": "DefinedTerm"
          }, 
          {
            "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/0914", 
            "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
            "name": "Resources Engineering and Extractive Metallurgy", 
            "type": "DefinedTerm"
          }
        ], 
        "author": [
          {
            "affiliation": {
              "alternateName": "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China", 
              "id": "http://www.grid.ac/institutes/grid.440785.a", 
              "name": [
                "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Cao", 
            "givenName": "Kai", 
            "id": "sg:person.010360415105.87", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.010360415105.87"
            ], 
            "type": "Person"
          }, 
          {
            "affiliation": {
              "alternateName": "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China", 
              "id": "http://www.grid.ac/institutes/grid.440785.a", 
              "name": [
                "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Shen", 
            "givenName": "Xiang-qian", 
            "id": "sg:person.0601655670.06", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0601655670.06"
            ], 
            "type": "Person"
          }, 
          {
            "affiliation": {
              "alternateName": "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China", 
              "id": "http://www.grid.ac/institutes/grid.440785.a", 
              "name": [
                "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Jing", 
            "givenName": "Mao-xiang", 
            "id": "sg:person.01162236364.13", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01162236364.13"
            ], 
            "type": "Person"
          }, 
          {
            "affiliation": {
              "alternateName": "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China", 
              "id": "http://www.grid.ac/institutes/grid.440785.a", 
              "name": [
                "School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Zhou", 
            "givenName": "Jian-xin", 
            "id": "sg:person.014673144705.58", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.014673144705.58"
            ], 
            "type": "Person"
          }
        ], 
        "citation": [
          {
            "id": "sg:pub.10.1023/a:1019648731836", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1011608322", 
              "https://doi.org/10.1023/a:1019648731836"
            ], 
            "type": "CreativeWork"
          }, 
          {
            "id": "sg:pub.10.1361/105994900770346042", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1027344144", 
              "https://doi.org/10.1361/105994900770346042"
            ], 
            "type": "CreativeWork"
          }, 
          {
            "id": "sg:pub.10.1007/s11771-004-0077-3", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1044565573", 
              "https://doi.org/10.1007/s11771-004-0077-3"
            ], 
            "type": "CreativeWork"
          }, 
          {
            "id": "sg:pub.10.1023/a:1004826324526", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1002579327", 
              "https://doi.org/10.1023/a:1004826324526"
            ], 
            "type": "CreativeWork"
          }, 
          {
            "id": "sg:pub.10.1007/s11771-007-0057-5", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1016383304", 
              "https://doi.org/10.1007/s11771-007-0057-5"
            ], 
            "type": "CreativeWork"
          }, 
          {
            "id": "sg:pub.10.1023/a:1004784720338", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1047127649", 
              "https://doi.org/10.1023/a:1004784720338"
            ], 
            "type": "CreativeWork"
          }
        ], 
        "datePublished": "2007-10-01", 
        "datePublishedReg": "2007-10-01", 
        "description": "The organic gel-thermal reduction process was used for the preparation of ferromagnetic metal Ni, Co and Fe fine fibers from the raw materials of citric acid, lactic acid and metal salts. The structure, thermal decomposition process and morphologies of the gel precursors and fibers derived from thermal reduction of these gel precursors were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, thermo-gravimetric/differential scanning calorimetry and scanning electron microscopy. The results show that spinnability of gel largely depends on molecular structure of metal-carboxylate complex that is a linear-type structure formed in the gel. As a result, the gels exhibit a good spinnability. Metal Ni, Co and Fe fine fibers are featured with diameters of around 1 \u03bcm and a high aspect ratio up to 1 \u00d7 106.", 
        "genre": "article", 
        "id": "sg:pub.10.1007/s11771-007-0116-y", 
        "inLanguage": "en", 
        "isAccessibleForFree": false, 
        "isPartOf": [
          {
            "id": "sg:journal.1381416", 
            "issn": [
              "2095-2899", 
              "2227-5223"
            ], 
            "name": "Journal of Central South University", 
            "publisher": "Springer Nature", 
            "type": "Periodical"
          }, 
          {
            "issueNumber": "5", 
            "type": "PublicationIssue"
          }, 
          {
            "type": "PublicationVolume", 
            "volumeNumber": "14"
          }
        ], 
        "keywords": [
          "gel precursors", 
          "reduction process", 
          "metal Ni", 
          "metal carboxylate complexes", 
          "ferromagnetic metal Ni", 
          "differential scanning calorimetry", 
          "thermal decomposition process", 
          "metal salts", 
          "scanning electron microscopy", 
          "molecular structure", 
          "linear type structure", 
          "ray diffraction", 
          "Fourier transform", 
          "scanning calorimetry", 
          "thermal reduction", 
          "high aspect ratio", 
          "fine fibers", 
          "citric acid", 
          "good spinnability", 
          "electron microscopy", 
          "gel", 
          "decomposition process", 
          "raw materials", 
          "aspect ratio", 
          "CO", 
          "spinnability", 
          "precursors", 
          "preparation", 
          "Ni", 
          "acid", 
          "spectroscopy", 
          "structure", 
          "diffraction", 
          "calorimetry", 
          "salt", 
          "complexes", 
          "lactic acid", 
          "fibers", 
          "transform", 
          "microscopy", 
          "thermo", 
          "morphology", 
          "materials", 
          "process", 
          "diameter", 
          "results", 
          "ratio", 
          "reduction"
        ], 
        "name": "Preparation of ferromagnetic metal fine fibers by organic gel-thermal reduction process", 
        "pagination": "607-611", 
        "productId": [
          {
            "name": "dimensions_id", 
            "type": "PropertyValue", 
            "value": [
              "pub.1046638547"
            ]
          }, 
          {
            "name": "doi", 
            "type": "PropertyValue", 
            "value": [
              "10.1007/s11771-007-0116-y"
            ]
          }
        ], 
        "sameAs": [
          "https://doi.org/10.1007/s11771-007-0116-y", 
          "https://app.dimensions.ai/details/publication/pub.1046638547"
        ], 
        "sdDataset": "articles", 
        "sdDatePublished": "2022-05-20T07:24", 
        "sdLicense": "https://scigraph.springernature.com/explorer/license/", 
        "sdPublisher": {
          "name": "Springer Nature - SN SciGraph project", 
          "type": "Organization"
        }, 
        "sdSource": "s3://com-springernature-scigraph/baseset/20220519/entities/gbq_results/article/article_442.jsonl", 
        "type": "ScholarlyArticle", 
        "url": "https://doi.org/10.1007/s11771-007-0116-y"
      }
    ]
     

    Download the RDF metadata as:  json-ld nt turtle xml License info

    HOW TO GET THIS DATA PROGRAMMATICALLY:

    JSON-LD is a popular format for linked data which is fully compatible with JSON.

    curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/s11771-007-0116-y'

    N-Triples is a line-based linked data format ideal for batch operations.

    curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/s11771-007-0116-y'

    Turtle is a human-readable linked data format.

    curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/s11771-007-0116-y'

    RDF/XML is a standard XML format for linked data.

    curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/s11771-007-0116-y'


     

    This table displays all metadata directly associated to this object as RDF triples.

    151 TRIPLES      22 PREDICATES      79 URIs      65 LITERALS      6 BLANK NODES

    Subject Predicate Object
    1 sg:pub.10.1007/s11771-007-0116-y schema:about anzsrc-for:09
    2 anzsrc-for:0914
    3 schema:author Ne7e4bbe747974f31a76442d90cf6c490
    4 schema:citation sg:pub.10.1007/s11771-004-0077-3
    5 sg:pub.10.1007/s11771-007-0057-5
    6 sg:pub.10.1023/a:1004784720338
    7 sg:pub.10.1023/a:1004826324526
    8 sg:pub.10.1023/a:1019648731836
    9 sg:pub.10.1361/105994900770346042
    10 schema:datePublished 2007-10-01
    11 schema:datePublishedReg 2007-10-01
    12 schema:description The organic gel-thermal reduction process was used for the preparation of ferromagnetic metal Ni, Co and Fe fine fibers from the raw materials of citric acid, lactic acid and metal salts. The structure, thermal decomposition process and morphologies of the gel precursors and fibers derived from thermal reduction of these gel precursors were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, thermo-gravimetric/differential scanning calorimetry and scanning electron microscopy. The results show that spinnability of gel largely depends on molecular structure of metal-carboxylate complex that is a linear-type structure formed in the gel. As a result, the gels exhibit a good spinnability. Metal Ni, Co and Fe fine fibers are featured with diameters of around 1 μm and a high aspect ratio up to 1 × 106.
    13 schema:genre article
    14 schema:inLanguage en
    15 schema:isAccessibleForFree false
    16 schema:isPartOf N30bb855c9a824fdb9270f2da42759208
    17 Nd57350b3dcb34702ab80db55486b1717
    18 sg:journal.1381416
    19 schema:keywords CO
    20 Fourier transform
    21 Ni
    22 acid
    23 aspect ratio
    24 calorimetry
    25 citric acid
    26 complexes
    27 decomposition process
    28 diameter
    29 differential scanning calorimetry
    30 diffraction
    31 electron microscopy
    32 ferromagnetic metal Ni
    33 fibers
    34 fine fibers
    35 gel
    36 gel precursors
    37 good spinnability
    38 high aspect ratio
    39 lactic acid
    40 linear type structure
    41 materials
    42 metal Ni
    43 metal carboxylate complexes
    44 metal salts
    45 microscopy
    46 molecular structure
    47 morphology
    48 precursors
    49 preparation
    50 process
    51 ratio
    52 raw materials
    53 ray diffraction
    54 reduction
    55 reduction process
    56 results
    57 salt
    58 scanning calorimetry
    59 scanning electron microscopy
    60 spectroscopy
    61 spinnability
    62 structure
    63 thermal decomposition process
    64 thermal reduction
    65 thermo
    66 transform
    67 schema:name Preparation of ferromagnetic metal fine fibers by organic gel-thermal reduction process
    68 schema:pagination 607-611
    69 schema:productId N38bf64a755254ef5b9a395eb4d93d0cc
    70 N9b60236e5f434fbfb725764b533cd672
    71 schema:sameAs https://app.dimensions.ai/details/publication/pub.1046638547
    72 https://doi.org/10.1007/s11771-007-0116-y
    73 schema:sdDatePublished 2022-05-20T07:24
    74 schema:sdLicense https://scigraph.springernature.com/explorer/license/
    75 schema:sdPublisher N02942d5e0f43488c89db45181759da39
    76 schema:url https://doi.org/10.1007/s11771-007-0116-y
    77 sgo:license sg:explorer/license/
    78 sgo:sdDataset articles
    79 rdf:type schema:ScholarlyArticle
    80 N02942d5e0f43488c89db45181759da39 schema:name Springer Nature - SN SciGraph project
    81 rdf:type schema:Organization
    82 N227a54aac2f84197a5be556ecb2b2595 rdf:first sg:person.014673144705.58
    83 rdf:rest rdf:nil
    84 N30bb855c9a824fdb9270f2da42759208 schema:volumeNumber 14
    85 rdf:type schema:PublicationVolume
    86 N38bf64a755254ef5b9a395eb4d93d0cc schema:name dimensions_id
    87 schema:value pub.1046638547
    88 rdf:type schema:PropertyValue
    89 N58e60b2e85024388a1ef96615e1a0bc4 rdf:first sg:person.0601655670.06
    90 rdf:rest Nf134849fda5e419aa6dc879d33488df3
    91 N9b60236e5f434fbfb725764b533cd672 schema:name doi
    92 schema:value 10.1007/s11771-007-0116-y
    93 rdf:type schema:PropertyValue
    94 Nd57350b3dcb34702ab80db55486b1717 schema:issueNumber 5
    95 rdf:type schema:PublicationIssue
    96 Ne7e4bbe747974f31a76442d90cf6c490 rdf:first sg:person.010360415105.87
    97 rdf:rest N58e60b2e85024388a1ef96615e1a0bc4
    98 Nf134849fda5e419aa6dc879d33488df3 rdf:first sg:person.01162236364.13
    99 rdf:rest N227a54aac2f84197a5be556ecb2b2595
    100 anzsrc-for:09 schema:inDefinedTermSet anzsrc-for:
    101 schema:name Engineering
    102 rdf:type schema:DefinedTerm
    103 anzsrc-for:0914 schema:inDefinedTermSet anzsrc-for:
    104 schema:name Resources Engineering and Extractive Metallurgy
    105 rdf:type schema:DefinedTerm
    106 sg:journal.1381416 schema:issn 2095-2899
    107 2227-5223
    108 schema:name Journal of Central South University
    109 schema:publisher Springer Nature
    110 rdf:type schema:Periodical
    111 sg:person.010360415105.87 schema:affiliation grid-institutes:grid.440785.a
    112 schema:familyName Cao
    113 schema:givenName Kai
    114 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.010360415105.87
    115 rdf:type schema:Person
    116 sg:person.01162236364.13 schema:affiliation grid-institutes:grid.440785.a
    117 schema:familyName Jing
    118 schema:givenName Mao-xiang
    119 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01162236364.13
    120 rdf:type schema:Person
    121 sg:person.014673144705.58 schema:affiliation grid-institutes:grid.440785.a
    122 schema:familyName Zhou
    123 schema:givenName Jian-xin
    124 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.014673144705.58
    125 rdf:type schema:Person
    126 sg:person.0601655670.06 schema:affiliation grid-institutes:grid.440785.a
    127 schema:familyName Shen
    128 schema:givenName Xiang-qian
    129 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0601655670.06
    130 rdf:type schema:Person
    131 sg:pub.10.1007/s11771-004-0077-3 schema:sameAs https://app.dimensions.ai/details/publication/pub.1044565573
    132 https://doi.org/10.1007/s11771-004-0077-3
    133 rdf:type schema:CreativeWork
    134 sg:pub.10.1007/s11771-007-0057-5 schema:sameAs https://app.dimensions.ai/details/publication/pub.1016383304
    135 https://doi.org/10.1007/s11771-007-0057-5
    136 rdf:type schema:CreativeWork
    137 sg:pub.10.1023/a:1004784720338 schema:sameAs https://app.dimensions.ai/details/publication/pub.1047127649
    138 https://doi.org/10.1023/a:1004784720338
    139 rdf:type schema:CreativeWork
    140 sg:pub.10.1023/a:1004826324526 schema:sameAs https://app.dimensions.ai/details/publication/pub.1002579327
    141 https://doi.org/10.1023/a:1004826324526
    142 rdf:type schema:CreativeWork
    143 sg:pub.10.1023/a:1019648731836 schema:sameAs https://app.dimensions.ai/details/publication/pub.1011608322
    144 https://doi.org/10.1023/a:1019648731836
    145 rdf:type schema:CreativeWork
    146 sg:pub.10.1361/105994900770346042 schema:sameAs https://app.dimensions.ai/details/publication/pub.1027344144
    147 https://doi.org/10.1361/105994900770346042
    148 rdf:type schema:CreativeWork
    149 grid-institutes:grid.440785.a schema:alternateName School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China
    150 schema:name School of Materials Science and Engineering, Jiangsu University, 212013, Zhenjiang, China
    151 rdf:type schema:Organization
     




    Preview window. Press ESC to close (or click here)


    ...