Monitoring a progressing transesterification reaction by fiber-optic near infrared spectroscopy with correlation to 1H nuclear magnetic resonance spectroscopy View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2000-05

AUTHORS

Gerhard Knothe

ABSTRACT

Biodiesel is a promising alternative diesel fuel obtained from vegetable oils, animal fats, or waste oils by transesterifying the oil or fat with an alcohol such as methanol. In an extension of previous work, fiber-optic near infrared spectroscopy was used to quantitatively monitor the transesterification reaction (6-L scale) of a vegetable oil (soybean oil) to methyl soyate. The results were correlated with 1H nuclear magnetic resonance spectroscopy. The method described here can be applied to the transesterification of other vegetable oils. More... »

PAGES

489-493

References to SciGraph publications

  • 1996-04. Simultaneous gas chromatographic determination of methanol and free glycerol in biodiesel in CHROMATOGRAPHIA
  • 1971-07. Near IR spectra of long chain vinyl derivatives in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1996-01. Measurement of free glycerol in biofuels in ANALYTICAL AND BIOANALYTICAL CHEMISTRY
  • 1997-11. Kinetics of transesterification of soybean oil in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1986-10. Transesterification kinetics of soybean oil 1 in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1994-12. Quality control of rapeseed oil methyl esters by determination of acyl conversion in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1995-10. 1H nuclear magnetic resonance determination of the yield of the transesterification of rapeseed oil with methanol in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1984-10. Variables affecting the yields of fatty esters from transesterified vegetable oils in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1993-12. Diesel fuel derived from vegetable oils, V [1]: Gas chromatographic determination of free glycerol in transesterified vegetable oils in CHROMATOGRAPHIA
  • 1986-10. Quantitation in the analysis of transesterified soybean oil by capillary gas chromatography 1 in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1999-07. Rapid monitoring of transesterification and assessing biodiesel fuel quality by near-infrared spectroscopy using a fiber-optic probe in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1995-11. Transesterification processes for vegetable oils: A simple control method of methyl ester content in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s11746-000-0078-5

    DOI

    http://dx.doi.org/10.1007/s11746-000-0078-5

    DIMENSIONS

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