Wettability and Reactivity of ZrB2 Substrates with Liquid Al View Full Text


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Article Info

DATE

2016-01-28

AUTHORS

R. Nowak, N. Sobczak, G. Bruzda, J. Wojewoda-Budka, L. Litynska-Dobrzynska, M. Homa, I. Kaban, L. Xi, L. Jaworska

ABSTRACT

Wetting characteristics of the Al/ZrB2 system were experimentally determined by the sessile drop method with application of separate heating of the ZrB2 and Al samples and combined with in situ cleaning of Al drop from native oxide film directly in vacuum chamber. The tests were performed in ultrahigh vacuum of 10−6 mbar at temperatures 710, 800, and 900 °C as well as in flowing inert gas (Ar) atmosphere at 1400 °C. The results evidenced that liquid Al does not wet ZrB2 substrate at 710 and 800 °C, forming high contact angles (θ) of 128° and 120°, respectively. At 900 °C, wetting phenomenon (θ < 90°) occurs in 29th minute and the contact angle decreases monotonically to the final value of 80°. At 1400 °C, wetting takes place immediately after drop deposition with a fast decrease in the contact angle to 76°. The solidified Al/ZrB2 couples were studied by scanning and transmission electron microscopy coupled with x-ray energy diffraction spectroscopy. Structural characterization revealed that only in the Al/ZrB2 couple produced at the highest temperature of 1400 °C new phases (Al3Zr, AlB2 and α-Al2O3) were formed. More... »

PAGES

3310-3316

References to SciGraph publications

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  • 2007-06-07. Ni-Zr (Nickel-Zirconium) in JOURNAL OF PHASE EQUILIBRIA AND DIFFUSION
  • 2005-04. Al-B-Ti (Aluminum-Boron-Titanium) in JOURNAL OF PHASE EQUILIBRIA AND DIFFUSION
  • 2014-01-09. On the Solubility of Group IV Elements (Ti, Zr, Hf) in Liquid Aluminum Below 800°C in JOURNAL OF PHASE EQUILIBRIA AND DIFFUSION
  • 2012-01-17. Control of Interfacial Reactivity Between ZrB2 and Ni-Based Brazing Alloys in JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
  • 1986-08. Age hardening of rapidly quenched Al-Zr-B alloys in JOURNAL OF MATERIALS SCIENCE
  • 2015-01-24. High-temperature wetting and interfacial interaction between liquid Al and TiB2 ceramic in JOURNAL OF MATERIALS SCIENCE
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    http://scigraph.springernature.com/pub.10.1007/s11665-016-1909-7

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    http://dx.doi.org/10.1007/s11665-016-1909-7

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    https://app.dimensions.ai/details/publication/pub.1015369491


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