Phase Evolution During the Carbothermic Reduction Process of Ilmenite Concentrate View Full Text


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Article Info

DATE

2015-02

AUTHORS

Hai-Peng Gou, Guo-Hua Zhang, Kuo-Chih Chou

ABSTRACT

The phase evolution during the carbothermic reduction process of Panzhihua ilmenite concentrate was investigated under argon atmosphere. The Panzhihua ilmenite concentrate briquette with graphite powder was reduced at 1473 K, 1573 K, 1673 K, and 1773 K (1200 °C, 1300 °C, 1400 °C, and 1500 °C) respectively, with the molar ratios of C to FeTiO3 being 4:1 and 5:1. The phase transformation of the briquette reduced at different temperatures was investigated by X-ray diffraction and scanning electron microscope. During the carbothermic reduction process from 1473 K to 1773 K (1200 °C to 1500 °C), it was found that main phases were Fe, Ti3O5, Ti2O3, and TiCxOy. The lowest temperature for the generation of TiCxOy was 1573 K (1300 °C) for both kinds of briquettes with different C contents. The rate controlling step for the carbothermic reduction above 1573 K (1300 °C) obeyed the diffusion model. The reduction degree of the ilmenite was increased by increasing the temperature. With the increase of reaction temperature and reaction time, TiCxOy phase would be reduced to TiC phase. More... »

PAGES

48-56

References to SciGraph publications

  • 1995-05. Simultaneous reduction and carburization of ilmenite in METALLURGICAL AND MATERIALS TRANSACTIONS B
  • 1999-12. Carbothermic reduction of llmenite (FeTiO3) and rutile (TiO2) in METALLURGICAL AND MATERIALS TRANSACTIONS B
  • 1980-10. Solid-liquid interfacial energies in binary and pseudo-binary systems in JOURNAL OF MATERIALS SCIENCE
  • 1970-06. Kinetics and mechanism of llmenite reduction with graphite in NONE
  • 1987-12. Kinetics of reduction of ilmenite with graphite at 1000 to 1100 °C in METALLURGICAL TRANSACTIONS B
  • 1998-10. Formation of TiN/TiC-Fe composites from ilmenite (FeTiO3) concentrate in METALLURGICAL AND MATERIALS TRANSACTIONS B
  • 1989-10. The influence of weathering on the reduction of llmenite with carbon in METALLURGICAL TRANSACTIONS B
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    http://scigraph.springernature.com/pub.10.1007/s11663-014-0175-z

    DOI

    http://dx.doi.org/10.1007/s11663-014-0175-z

    DIMENSIONS

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