Crystal structures and other properties of ephedrone (methcathinone) hydrochloride, N-acetylephedrine and N-acetylephedrone View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2019-01

AUTHORS

Piotr Kuś, Hubert Hellwig, Joachim Kusz, Maria Książek, Marcin Rojkiewicz, Aleksander Sochanik

ABSTRACT

Purpose: Three compounds obtained from ephedrine were identified and characterized by various instrumental analytical methods. Ephedrone (methcathinone) hydrochloride and its fundamental derivatives N-acetylephedrine and N-acetylephedrone were analyzed as precursors of a cathinone derivative. Methods: The obtained samples were analyzed by gas chromatography coupled with mass spectrometry, nuclear magnetic resonance spectroscopy, infrared and Raman spectroscopy, and X-ray crystallography. Results: The three compounds were confirmed as: N-methyl-2-amino-1-phenylpropan-1-one (methcathinone) hydrochloride, N-acetyl-N-methyl-2-amino-1-phenylpropan-1-one (cathinone derivative), and N-acetyl-N-methyl-2-amino-1-phenylpropan-1-ol (acetyl derivative of ephedrine). Conclusions: X-ray crystallography is especially useful for identifying the new designer drugs and their different precursor forms. More... »

PAGES

224-230

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11419-018-0436-7

DOI

http://dx.doi.org/10.1007/s11419-018-0436-7

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1106224974

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30636989


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