Hydrogenation Processes at the Surface of Ruthenium Nanoparticles: A NMR Study View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-09

AUTHORS

I. Favier, P. Lavedan, S. Massou, E. Teuma, K. Philippot, B. Chaudret, M. Gómez

ABSTRACT

The reactivity of ruthenium nanoparticles stabilized by 4-(3-phenylpropyl)pyridine in hydrogen transfer and hydrogenation processes was monitored by NMR spectroscopy. Unsaturated substrates such as styrene, 4-vinylpyridine and 4-phenyl-but-3-en-2-one were used as model molecules to investigate the surface properties of nanoparticles by a combination of NMR studies. Interestingly, the hydrides present at the metallic surface after nanoparticles synthesis are selectively transferred to vinylic groups without reducing the aromatic rings, under dihydrogen-free atmosphere. DOSY and NOE NMR experiments permitted to propose a way of interaction of the organic compounds at the metallic surface. In particular, the coordination of the substrate could be evidenced for 4-vinylpyridine and 4-ethylpyridine but not for styrene derivatives. Curved double arrows represent magnetization exchanges. Straight arrows represent adsorption/desorption phenomena. More... »

PAGES

1253-1261

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11244-013-0092-4

DOI

http://dx.doi.org/10.1007/s11244-013-0092-4

DIMENSIONS

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