Mixed phosphine/N-heterocyclic carbene–palladium complexes: synthesis, characterization, crystal structure and application in the Sonogashira reaction in aqueous media View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-04

AUTHORS

Aydın Aktaş, Fatoş Erdemir, Duygu Barut Celepci, Yetkin Gök, Muhittin Aygün

ABSTRACT

A series of 2-hydroxyethyl-substituted N-heterocyclic carbene–(NHC)PdX2PPh3 complexes have been synthesized by substitution of the pyridine or 3-chloropyridine ligand in (NHC)PdX2(pyridine/3-chloropyridine) complexes with triphenylphosphine. The new complexes were characterized by 1H, 13C {1H}, 31P {1H}NMR, FTIR spectroscopy and elemental analysis. Also, the molecular and crystal structures of 1c and 1d have been obtained by single-crystal X-ray diffraction. The 2-hydroxyethyl-substituted (NHC)PdX2PPh3 complexes have been examined as catalysts for the Sonogashira cross-coupling reaction in water/DMF solvent mixtures. More... »

PAGES

229-236

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11243-018-0286-5

DOI

http://dx.doi.org/10.1007/s11243-018-0286-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1109759461


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