Synthesis and characterization of Mn(II) and Zn(II) azido complexes with halo-substituted pyridine derivative ligands View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-04

AUTHORS

Franz A. Mautner, Beate Sudy, Alshima’a A. Massoud, Morsy A. M. Abu-Youssef

ABSTRACT

The synthesis, IR spectra and single-crystal structures of two Mn(II) and one Zn(II) azido complexes with halo-substituted pyridine derivative ligands are reported: [Mn(N3)-2(3-Brpy)2(H2O)]2(3-Brpy)2 (1), [Mn(N3)2(3-Brpy)2]n (2) and [Zn(N3)2(3-amino,2-chloropyridine)]n (3) with 3-Brpy = 3-bromopyridine. In the dinuclear Mn(II) complex 1 and polymeric 1D Zn(II) complex 3, di-EO only azido bridges exist, whereas in the polymeric Mn(II) 1D system of 2, a rather less common di-EO/di-EO/di-EE azido bridging sequence has been observed (EO = end-on, EE = end-to-end). The halo-substituted pyridine derivatives act in the three compounds as terminal ligands and in 1 also as solvent molecules. More... »

PAGES

319-325

Journal

TITLE

Transition Metal Chemistry

ISSUE

3

VOLUME

38

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11243-013-9696-6

DOI

http://dx.doi.org/10.1007/s11243-013-9696-6

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1042205190


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