A selenium-bonded oxorhenium(V) complex: solvothermal synthesis, structural characterization, and electrochemical behavior View Full Text


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Article Info

DATE

2011-09

AUTHORS

Biswajit Das, Rajesh Chakraborty, Sandipan Sarkar, Ennio Zangrando, Pabitra Chattopadhyay

ABSTRACT

The solvothermal reaction of [ReOCl3(PPh3)2] with 2,2′-seleno-bis(4,6-di-tert-butylphenol) (H2L1) in ethanol at 95 °C resulted in an oxorhenium(V) complex of formulation [ReO(L1)(L2)] due to the in situ formation of 2-selenochloromethyl-4,6-di-tert-butylphenolate (L2) through the cleavage of one C–Se bond of H2L1. The mononuclear oxorhenium(V) complex was characterized by physicochemical and spectroscopic methods along with detailed structural analysis by single crystal X-ray crystallography. Electrochemical studies revealed a one-electron equivalent quasi-reversible voltammogram for the ReO(V)/ReO(VI) redox couple at 1.28 V (versus SCE) with no cathodic response for ReO(V) → ReO(IV) reduction. More... »

PAGES

663

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11243-011-9516-9

DOI

http://dx.doi.org/10.1007/s11243-011-9516-9

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