Synthesis and spatial structure of new chiral dopants from allobetuline series for cholesteric liquid-crystal compositions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-02

AUTHORS

Nikolay L. Babak, Oleg V. Shishkin, Svitlana V. Shishkina, Ivan M. Gella, Vladimir I. Musatov, Nataliya B. Novikova, Victoria V. Lipson

ABSTRACT

New series of chiral dopants for cholesteric liquid-crystal compositions were synthesized on the base of 2-substituted allobetuline derivatives, and their steric structure was determined by X-ray analysis. The relationship between spatial structure of these compounds and their ability to induce cholesteric helix in 4-pentyl-4′-cyanobiphenyl nematic solvent was examined. The highest values of the helical twisting power |β| (71.38 ± 3.4) and (84.25 ± 3.7) mkm−1 mol·pats−1 showed (E)-2-(4-chlorophenylmethylidene)-allobetuline and (2R,3R)-3-(4′-chlorophenyl)-2,2′-spiro-oxyranoallobetuline correspondingly. How the value of |β| in this series of compounds varies depending on the spatial arrangement relative to the aryl moiety of the chiral core is shown. More... »

PAGES

295-303

Journal

TITLE

Structural Chemistry

ISSUE

1

VOLUME

27

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11224-015-0700-y

DOI

http://dx.doi.org/10.1007/s11224-015-0700-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1045461126


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