X-ray crystal structures and conformational analysis of cyclic acetals derived from tartaric acid and rigid spacer units View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-08

AUTHORS

Diana Eißmann, Felix Katzsch, Edwin Weber

ABSTRACT

Three tartaric ester and tartaric acid derivatives (1–3) with the hydroxy groups being linked via cyclic acetal (1,3-dioxolane) formation to a rigid core, containing phenyl and ethynyl units, have been synthesized. Their crystal structures are reported, emphasizing the molecular geometry, intermolecular interactions, and the resulting packing motifs. All dioxolane rings present in the crystal structures of 1–3 are analyzed and compared with regard to their conformational behavior. In spite of similar substitution patterns, the dioxolane units adopt different conformations including twist and varying envelope isomers. The crystal structures are dominated by C–H···O (esters 1 and 2) and O–H···O (acid 3) hydrogen bonds, leading to different types of packing motifs being characteristic of strand and layer formation. More... »

PAGES

1131-1142

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11224-011-9934-5

DOI

http://dx.doi.org/10.1007/s11224-011-9934-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1024105217


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