X-Ray Powder Diffraction as a Tool to Investigate the Ultrastructure of Nanoparticles View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-02-08

AUTHORS

O. Prymak, S. Ristig, V. Meyer-Zaika, A. Rostek, L. Ruiz, J. M. González-Calbet, M. Vallet-Regi, M. Epple

ABSTRACT

The potential of x-ray powder diffraction to analyze the size and ultrastructure of metallic nanoparticles (silver, gold, silver-gold alloy, and calcium phosphate) is demonstrated. By the Rietveld analysis, it is possible to estimate the crystallite size for such nanoparticles, even if they are very small (4 nm), using the effect of peak broadening in small crystallites. The results correspond well to crystallite size as determined by transmission electron microscopy (TEM), also confirming the twinned nature of the metallic nanoparticles. For calcium phosphate nanorods which are not twinned, the results by x-ray powder diffraction and TEM are in good agreement. More... »

PAGES

1111-1115

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11182-014-0149-2

DOI

http://dx.doi.org/10.1007/s11182-014-0149-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1004708036


Indexing Status Check whether this publication has been indexed by Scopus and Web Of Science using the SN Indexing Status Tool
Incoming Citations Browse incoming citations for this publication using opencitations.net

JSON-LD is the canonical representation for SciGraph data.

TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

[
  {
    "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
    "about": [
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/10", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Technology", 
        "type": "DefinedTerm"
      }, 
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/1007", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Nanotechnology", 
        "type": "DefinedTerm"
      }
    ], 
    "author": [
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Prymak", 
        "givenName": "O.", 
        "id": "sg:person.0725371511.49", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0725371511.49"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Ristig", 
        "givenName": "S.", 
        "id": "sg:person.012247406333.68", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.012247406333.68"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Meyer-Zaika", 
        "givenName": "V.", 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Rostek", 
        "givenName": "A.", 
        "id": "sg:person.01317761023.35", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01317761023.35"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "School of Engineering Design, Valencia, Spain", 
          "id": "http://www.grid.ac/institutes/None", 
          "name": [
            "School of Engineering Design, Valencia, Spain"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Ruiz", 
        "givenName": "L.", 
        "id": "sg:person.0576256671.08", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0576256671.08"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Department of Inorganic and Bioinorganic Chemistry, Universidad Complutense de Madrid, Madrid, Spain", 
          "id": "http://www.grid.ac/institutes/grid.4795.f", 
          "name": [
            "Department of Inorganic and Bioinorganic Chemistry, Universidad Complutense de Madrid, Madrid, Spain"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Gonz\u00e1lez-Calbet", 
        "givenName": "J. M.", 
        "id": "sg:person.016437315754.70", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.016437315754.70"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Vallet-Regi", 
        "givenName": "M.", 
        "id": "sg:person.01262725302.26", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01262725302.26"
        ], 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany", 
          "id": "http://www.grid.ac/institutes/grid.5718.b", 
          "name": [
            "Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Epple", 
        "givenName": "M.", 
        "id": "sg:person.011342402346.80", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.011342402346.80"
        ], 
        "type": "Person"
      }
    ], 
    "citation": [
      {
        "id": "sg:pub.10.1007/s11051-012-1153-5", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1008977049", 
          "https://doi.org/10.1007/s11051-012-1153-5"
        ], 
        "type": "CreativeWork"
      }
    ], 
    "datePublished": "2014-02-08", 
    "datePublishedReg": "2014-02-08", 
    "description": "The potential of x-ray powder diffraction to analyze the size and ultrastructure of metallic nanoparticles (silver, gold, silver-gold alloy, and calcium phosphate) is demonstrated. By the Rietveld analysis, it is possible to estimate the crystallite size for such nanoparticles, even if they are very small (4\u00a0nm), using the effect of peak broadening in small crystallites. The results correspond well to crystallite size as determined by transmission electron microscopy (TEM), also confirming the twinned nature of the metallic nanoparticles. For calcium phosphate nanorods which are not twinned, the results by x-ray powder diffraction and TEM are in good agreement.", 
    "genre": "article", 
    "id": "sg:pub.10.1007/s11182-014-0149-2", 
    "isAccessibleForFree": false, 
    "isPartOf": [
      {
        "id": "sg:journal.1313824", 
        "issn": [
          "1064-8887", 
          "1573-9228"
        ], 
        "name": "Russian Physics Journal", 
        "publisher": "Springer Nature", 
        "type": "Periodical"
      }, 
      {
        "issueNumber": "10", 
        "type": "PublicationIssue"
      }, 
      {
        "type": "PublicationVolume", 
        "volumeNumber": "56"
      }
    ], 
    "keywords": [
      "transmission electron microscopy", 
      "X-ray powder diffraction", 
      "metallic nanoparticles", 
      "powder diffraction", 
      "crystallite size", 
      "calcium phosphate nanorods", 
      "such nanoparticles", 
      "nanoparticles", 
      "electron microscopy", 
      "small crystallites", 
      "diffraction", 
      "nanorods", 
      "effect of peak", 
      "size", 
      "microscopy", 
      "Rietveld analysis", 
      "crystallites", 
      "potential", 
      "good agreement", 
      "peak", 
      "results", 
      "nature", 
      "tool", 
      "ultrastructure", 
      "effect", 
      "analysis", 
      "agreement"
    ], 
    "name": "X-Ray Powder Diffraction as a Tool to Investigate the Ultrastructure of Nanoparticles", 
    "pagination": "1111-1115", 
    "productId": [
      {
        "name": "dimensions_id", 
        "type": "PropertyValue", 
        "value": [
          "pub.1004708036"
        ]
      }, 
      {
        "name": "doi", 
        "type": "PropertyValue", 
        "value": [
          "10.1007/s11182-014-0149-2"
        ]
      }
    ], 
    "sameAs": [
      "https://doi.org/10.1007/s11182-014-0149-2", 
      "https://app.dimensions.ai/details/publication/pub.1004708036"
    ], 
    "sdDataset": "articles", 
    "sdDatePublished": "2022-09-02T15:57", 
    "sdLicense": "https://scigraph.springernature.com/explorer/license/", 
    "sdPublisher": {
      "name": "Springer Nature - SN SciGraph project", 
      "type": "Organization"
    }, 
    "sdSource": "s3://com-springernature-scigraph/baseset/20220902/entities/gbq_results/article/article_648.jsonl", 
    "type": "ScholarlyArticle", 
    "url": "https://doi.org/10.1007/s11182-014-0149-2"
  }
]
 

Download the RDF metadata as:  json-ld nt turtle xml License info

HOW TO GET THIS DATA PROGRAMMATICALLY:

JSON-LD is a popular format for linked data which is fully compatible with JSON.

curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/s11182-014-0149-2'

N-Triples is a line-based linked data format ideal for batch operations.

curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/s11182-014-0149-2'

Turtle is a human-readable linked data format.

curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/s11182-014-0149-2'

RDF/XML is a standard XML format for linked data.

curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/s11182-014-0149-2'


 

This table displays all metadata directly associated to this object as RDF triples.

142 TRIPLES      21 PREDICATES      52 URIs      43 LITERALS      6 BLANK NODES

Subject Predicate Object
1 sg:pub.10.1007/s11182-014-0149-2 schema:about anzsrc-for:10
2 anzsrc-for:1007
3 schema:author N0a067766284f4bd7913b67cb6d1deef6
4 schema:citation sg:pub.10.1007/s11051-012-1153-5
5 schema:datePublished 2014-02-08
6 schema:datePublishedReg 2014-02-08
7 schema:description The potential of x-ray powder diffraction to analyze the size and ultrastructure of metallic nanoparticles (silver, gold, silver-gold alloy, and calcium phosphate) is demonstrated. By the Rietveld analysis, it is possible to estimate the crystallite size for such nanoparticles, even if they are very small (4 nm), using the effect of peak broadening in small crystallites. The results correspond well to crystallite size as determined by transmission electron microscopy (TEM), also confirming the twinned nature of the metallic nanoparticles. For calcium phosphate nanorods which are not twinned, the results by x-ray powder diffraction and TEM are in good agreement.
8 schema:genre article
9 schema:isAccessibleForFree false
10 schema:isPartOf N1957d5fba8b145c99c82cef8cde41d81
11 Ne96e269fca2b4babb94e018c927c7d60
12 sg:journal.1313824
13 schema:keywords Rietveld analysis
14 X-ray powder diffraction
15 agreement
16 analysis
17 calcium phosphate nanorods
18 crystallite size
19 crystallites
20 diffraction
21 effect
22 effect of peak
23 electron microscopy
24 good agreement
25 metallic nanoparticles
26 microscopy
27 nanoparticles
28 nanorods
29 nature
30 peak
31 potential
32 powder diffraction
33 results
34 size
35 small crystallites
36 such nanoparticles
37 tool
38 transmission electron microscopy
39 ultrastructure
40 schema:name X-Ray Powder Diffraction as a Tool to Investigate the Ultrastructure of Nanoparticles
41 schema:pagination 1111-1115
42 schema:productId Nb67acd13050f4a21a91492d158e7889f
43 Nf5ce27a2f0684ab3be901f2950554585
44 schema:sameAs https://app.dimensions.ai/details/publication/pub.1004708036
45 https://doi.org/10.1007/s11182-014-0149-2
46 schema:sdDatePublished 2022-09-02T15:57
47 schema:sdLicense https://scigraph.springernature.com/explorer/license/
48 schema:sdPublisher Nf2c36da7bc59418ba561b109421cc40c
49 schema:url https://doi.org/10.1007/s11182-014-0149-2
50 sgo:license sg:explorer/license/
51 sgo:sdDataset articles
52 rdf:type schema:ScholarlyArticle
53 N0a067766284f4bd7913b67cb6d1deef6 rdf:first sg:person.0725371511.49
54 rdf:rest Nef3ced7d7a504012a42225e52e15a1d4
55 N0eb795171352473b9a3248b88a21823b rdf:first sg:person.0576256671.08
56 rdf:rest Na8e58aabcbdc41fbbfad0baec2744db0
57 N1957d5fba8b145c99c82cef8cde41d81 schema:volumeNumber 56
58 rdf:type schema:PublicationVolume
59 N40e155a3ab38482a891e5cc7836dc8c6 schema:affiliation grid-institutes:grid.5718.b
60 schema:familyName Meyer-Zaika
61 schema:givenName V.
62 rdf:type schema:Person
63 N98de5e389a0542269107b96ab521ff56 rdf:first sg:person.011342402346.80
64 rdf:rest rdf:nil
65 N9a8d1055ff7b441ea6f8046d30641052 rdf:first N40e155a3ab38482a891e5cc7836dc8c6
66 rdf:rest Ndf06c485fa1a4385ac0aa6157a3d2d80
67 Na8e58aabcbdc41fbbfad0baec2744db0 rdf:first sg:person.016437315754.70
68 rdf:rest Nfe4766b908b04a4498d88c6aa4fcfc15
69 Nb67acd13050f4a21a91492d158e7889f schema:name dimensions_id
70 schema:value pub.1004708036
71 rdf:type schema:PropertyValue
72 Ndf06c485fa1a4385ac0aa6157a3d2d80 rdf:first sg:person.01317761023.35
73 rdf:rest N0eb795171352473b9a3248b88a21823b
74 Ne96e269fca2b4babb94e018c927c7d60 schema:issueNumber 10
75 rdf:type schema:PublicationIssue
76 Nef3ced7d7a504012a42225e52e15a1d4 rdf:first sg:person.012247406333.68
77 rdf:rest N9a8d1055ff7b441ea6f8046d30641052
78 Nf2c36da7bc59418ba561b109421cc40c schema:name Springer Nature - SN SciGraph project
79 rdf:type schema:Organization
80 Nf5ce27a2f0684ab3be901f2950554585 schema:name doi
81 schema:value 10.1007/s11182-014-0149-2
82 rdf:type schema:PropertyValue
83 Nfe4766b908b04a4498d88c6aa4fcfc15 rdf:first sg:person.01262725302.26
84 rdf:rest N98de5e389a0542269107b96ab521ff56
85 anzsrc-for:10 schema:inDefinedTermSet anzsrc-for:
86 schema:name Technology
87 rdf:type schema:DefinedTerm
88 anzsrc-for:1007 schema:inDefinedTermSet anzsrc-for:
89 schema:name Nanotechnology
90 rdf:type schema:DefinedTerm
91 sg:journal.1313824 schema:issn 1064-8887
92 1573-9228
93 schema:name Russian Physics Journal
94 schema:publisher Springer Nature
95 rdf:type schema:Periodical
96 sg:person.011342402346.80 schema:affiliation grid-institutes:grid.5718.b
97 schema:familyName Epple
98 schema:givenName M.
99 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.011342402346.80
100 rdf:type schema:Person
101 sg:person.012247406333.68 schema:affiliation grid-institutes:grid.5718.b
102 schema:familyName Ristig
103 schema:givenName S.
104 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.012247406333.68
105 rdf:type schema:Person
106 sg:person.01262725302.26 schema:affiliation grid-institutes:grid.5718.b
107 schema:familyName Vallet-Regi
108 schema:givenName M.
109 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01262725302.26
110 rdf:type schema:Person
111 sg:person.01317761023.35 schema:affiliation grid-institutes:grid.5718.b
112 schema:familyName Rostek
113 schema:givenName A.
114 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01317761023.35
115 rdf:type schema:Person
116 sg:person.016437315754.70 schema:affiliation grid-institutes:grid.4795.f
117 schema:familyName González-Calbet
118 schema:givenName J. M.
119 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.016437315754.70
120 rdf:type schema:Person
121 sg:person.0576256671.08 schema:affiliation grid-institutes:None
122 schema:familyName Ruiz
123 schema:givenName L.
124 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0576256671.08
125 rdf:type schema:Person
126 sg:person.0725371511.49 schema:affiliation grid-institutes:grid.5718.b
127 schema:familyName Prymak
128 schema:givenName O.
129 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0725371511.49
130 rdf:type schema:Person
131 sg:pub.10.1007/s11051-012-1153-5 schema:sameAs https://app.dimensions.ai/details/publication/pub.1008977049
132 https://doi.org/10.1007/s11051-012-1153-5
133 rdf:type schema:CreativeWork
134 grid-institutes:None schema:alternateName School of Engineering Design, Valencia, Spain
135 schema:name School of Engineering Design, Valencia, Spain
136 rdf:type schema:Organization
137 grid-institutes:grid.4795.f schema:alternateName Department of Inorganic and Bioinorganic Chemistry, Universidad Complutense de Madrid, Madrid, Spain
138 schema:name Department of Inorganic and Bioinorganic Chemistry, Universidad Complutense de Madrid, Madrid, Spain
139 rdf:type schema:Organization
140 grid-institutes:grid.5718.b schema:alternateName Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany
141 schema:name Institute of Inorganic Chemistry and Center for Nanointegration Duisburg-Essen, University of Duisburg-Essen, Essen, Germany
142 rdf:type schema:Organization
 




Preview window. Press ESC to close (or click here)


...