Synthesis and Structure of 5-Indolyl-6-thienyl-1,2,4-triazines View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2005-06

AUTHORS

M. M. Krayushkin, V. N. Yarovenko, I. P. Sedishev, I. V. Zavarzin, L. G. Vorontsova, Z. A. Starikova

ABSTRACT

Acylation of indole and 2,5-dimethylthiophene with 2-(3-indolyl)-2-oxoacetyl chloride afforded the corresponding diketones. 1-(2,5-Dimethyl-3-thienyl)-2-(3-indolyl)ethanedione reacted with thiosemicarbazide under atmosperic and elevated pressure to give 6-(2,5-dimethyl-3-thienyl)-5-(3-indolyl)-2,3-dihydro-1,2,4-triazine-3-thione whose structure was studied in detail by the X-ray diffraction method. Reactions of 6-(2,5-dimethyl-3-thienyl)-5-(3-indolyl)-2,3-dihydro-1,2,4-triazine-3-thione with amines and hydrazine resulted in formation of fused triazolo- and tetrazolotriazines.

PAGES

875-883

Journal

TITLE

Russian Journal of Organic Chemistry

ISSUE

6

VOLUME

41

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s11178-005-0258-z

DOI

http://dx.doi.org/10.1007/s11178-005-0258-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1005576169


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